(3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER

Base Information

Chemical Name:(3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER
CAS No.:213032-75-8
Molecular Formula:C₁₂H₁₉O₅P
Molecular Weight:274.254
Hs Code.:
Mol file:213032-75-8.mol

Synonyms:(3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER

Suppliers and Price of (3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER 95.00%
5MG
$ 503.46

Total 2 raw suppliers

Chemical Property of (3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER

Chemical Property:

PSA：63.80000
LogP:2.59520

Purity/Quality:

97% ^*data from raw suppliers

(3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER

There total 5 articles about (3,4-DIMETHOXY-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 91-16-7
1,2-dimethoxybenzene

: 762-04-9
phosphonic acid diethyl ester

: 213032-75-8
diethyl (3,4-dimethoxyphenyl)phosphonate

Guidance literature:: With manganese(III) triacetate dihydrate; In acetic acid; at 60 ℃; for 5h;
DOI:10.1016/j.tetlet.2010.03.029

Reference yield: 67.0%

: 122775-35-3
3,4-Dimethoxyphenylboronic acid

: 762-04-9
phosphonic acid diethyl ester

: 213032-75-8
diethyl (3,4-dimethoxyphenyl)phosphonate

Guidance literature:: With 2.9-dimethyl-1,10-phenanthroline; palladium diacetate; p-benzoquinone; In N,N-dimethyl-formamide; at 100 ℃; for 0.5h; Microwave irradiation;
DOI:10.1002/chem.200901473

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 122-52-1
triethyl phosphite

: diethyl (2,3-dimethoxyphenyl)phosphonate

: 213032-75-8
diethyl (3,4-dimethoxyphenyl)phosphonate

Guidance literature:: With ammonium peroxydisulfate; tris(2,2′-bipyrazine-N1,N1′)ruthenium(II) hexafluorophosphate; In acetonitrile; at 25 ℃; for 20h; Overall yield = 99 %; Overall yield = 39.3 mg; regioselective reaction; Inert atmosphere; Irradiation;
DOI:10.1002/chem.201701283