alpha-D-Ribofuranoside, methyl 5-deoxy-5-[(1-oxo-2-propenyl)amino]- (9CI)

Base Information

Chemical Name:alpha-D-Ribofuranoside, methyl 5-deoxy-5-[(1-oxo-2-propenyl)amino]- (9CI)
CAS No.:656236-95-2
Molecular Formula:C9H15NO5
Molecular Weight:217.22
Hs Code.:
Mol file:656236-95-2.mol

Synonyms:alpha-D-Ribofuranoside, methyl 5-deoxy-5-[(1-oxo-2-propenyl)amino]- (9CI)

Suppliers and Price of alpha-D-Ribofuranoside, methyl 5-deoxy-5-[(1-oxo-2-propenyl)amino]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of alpha-D-Ribofuranoside, methyl 5-deoxy-5-[(1-oxo-2-propenyl)amino]- (9CI)

Chemical Property:

PSA：88.02000
LogP:-1.22740

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of alpha-D-Ribofuranoside, methyl 5-deoxy-5-[(1-oxo-2-propenyl)amino]- (9CI)

There total 4 articles about alpha-D-Ribofuranoside, methyl 5-deoxy-5-[(1-oxo-2-propenyl)amino]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 2051-76-5
acrylic acid anhydride

: 262600-85-1
5'-amino-5'-deoxy-1'-O-methyl-D-ribose

: 656236-95-2
5'-acrylamido-5'-deoxy-1'-O-methyl-D-ribose

Guidance literature:: In tetrahydrofuran; at 0 - 25 ℃; for 11.3h;
DOI:10.1039/b301166f

Reference yield:

: 52485-92-4
methyl α-D-ribofuranoside

: 656236-95-2
5'-acrylamido-5'-deoxy-1'-O-methyl-D-ribose

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / PPh₃; I₂; pyridine / dioxane / 24 h / 25 °C

2: 97 percent / NaN₃ / dimethylformamide / 24 h / 110 °C

3: 64 percent / PPh₃; H₂O / tetrahydrofuran / 24 h / 25 °C

4: 47 percent / tetrahydrofuran / 11.3 h / 0 - 25 °C

With pyridine; sodium azide; water; iodine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/b301166f

Reference yield:

: 656236-93-0
methyl 5-deoxy-5-iodo-α-D-riboside

: 656236-95-2
5'-acrylamido-5'-deoxy-1'-O-methyl-D-ribose

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaN₃ / dimethylformamide / 24 h / 110 °C

2: 64 percent / PPh₃; H₂O / tetrahydrofuran / 24 h / 25 °C

3: 47 percent / tetrahydrofuran / 11.3 h / 0 - 25 °C

With sodium azide; water; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b301166f