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Acrylic anhydride
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2-Propenoic acid,1,1'-anhydride 2051-76-5
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2051-76-5 Usage

Description

Acrylic anhydride is used to prepare specialty acrylate, acrylamide monomers. Forms cyclic anhydrides on polymerization and does not produce crosslinks in polymers. It is used in the preparation of acrylic resin. And it is also used in organic synthesis. For example: it can react with adamantan-1-ol to get acrylic acid adamantan-1-yl ester. This reaction needs catalytic agent acidic catalyst and solvent cyclohexane by heating. The yield is 95%.
InChI:InChI=1/C6H6O3/c1-3-5(7)9-6(8)4-2/h3-4H,1-2H2

2051-76-5SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Acrylic anhydride

1.2 Other means of identification

Product number -
Other names acryloyl anhydride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:2051-76-5 SDS

2051-76-5Synthetic route

acrylic acid
79-10-7

acrylic acid

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

Conditions
ConditionsYield
With trifluorormethanesulfonic acid; acetic anhydride at 100℃;95%
With triethylamine; benzenesulfonyl chloride; Santonox R; 2-(2-hydroxy-3-tert-butyl-5-methylbenzyl)-4-methyl-6-tert-butylphenyl acrylate; pentaerythritol tetrakis(β-dodecylmercapto)propionate In dichloromethane at 5 - 30℃; for 3h;91%
With methanesulfonyl chloride; triethylamine; Santonox R; 2-(2-hydroxy-3-tert-butyl-5-methylbenzyl)-4-methyl-6-tert-butylphenyl acrylate; pentaerythritol tetrakis(β-dodecylmercapto)propionate In dichloromethane at 5 - 30℃; for 3h;79%
potassium acrylate
10192-85-5

potassium acrylate

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

Conditions
ConditionsYield
With 10H-phenothiazine; methanesulfonyl chloride; 4-methoxy-phenol In acetone for 0.5h; Reagent/catalyst; Cooling with ice;93.3%
acrylic acid
79-10-7

acrylic acid

acryloyl chloride
814-68-6

acryloyl chloride

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 16.0833h; Inert atmosphere; Cooling with ice;80%
With triethylamine In tetrahydrofuran at 20℃; for 16h; Cooling with ice; Inert atmosphere;80%
With triethylamine In tetrahydrofuran at 20℃; for 16h;75%
acetic anhydride
108-24-7

acetic anhydride

acrylic acid
79-10-7

acrylic acid

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

Conditions
ConditionsYield
With phosphorus oic acid
With 10H-phenothiazine; cupric dibutyldithiocarbamate at 90℃; under 18 - 160 Torr; Product distribution / selectivity; Air atmosphere;
sodium 2-propenoate
7446-81-3

sodium 2-propenoate

acryloyl chloride
814-68-6

acryloyl chloride

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

acryloyl chloride
814-68-6

acryloyl chloride

Lithium acrylate
13270-28-5

Lithium acrylate

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 2h;
acryloyl chloride
814-68-6

acryloyl chloride

acrylacidic sodium

acrylacidic sodium

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

acrylic acid
79-10-7

acrylic acid

acetylene
74-86-2

acetylene

carbon monoxide

carbon monoxide

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

Conditions
ConditionsYield
With 1,2-dichloro-ethane; tetracarbonyl nickel
With 1,4-dioxane; tetracarbonyl nickel
With 1,4-dioxane; tetracarbonyl nickel
With 1,2-dichloro-ethane; tetracarbonyl nickel
acrylic acid
79-10-7

acrylic acid

acetylene
74-86-2

acetylene

tetracarbonyl nickel

tetracarbonyl nickel

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

Conditions
ConditionsYield
With 1,4-dioxane
With 1,2-dichloro-ethane
With 1,4-dioxane
With 1,2-dichloro-ethane
acetylene
74-86-2

acetylene

carbon monoxide

carbon monoxide

A

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

B

acrylic acid
79-10-7

acrylic acid

Conditions
ConditionsYield
With water; acetonitrile; nickel dibromide at 90℃; under 14710.2 Torr;
triethylamine
121-44-8

triethylamine

acrylic acid
79-10-7

acrylic acid

acryloyl chloride
814-68-6

acryloyl chloride

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

Conditions
ConditionsYield
In tetrahydrofuran
sodium 2-propenoate
7446-81-3

sodium 2-propenoate

benzoyl chloride
98-88-4

benzoyl chloride

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

acide 2-bromo-3-hydroxy propanoique
160732-12-7

acide 2-bromo-3-hydroxy propanoique

C6H7BrO4

C6H7BrO4

Conditions
ConditionsYield
With toluene-4-sulfonic acid; 2-hydroxyresorcinol at 25℃; for 12h; Darkness;99.8%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

N,N-bis(2-hydroxyethyl)octadeca-9,11,13-trienamide

N,N-bis(2-hydroxyethyl)octadeca-9,11,13-trienamide

C28H43NO5

C28H43NO5

Conditions
ConditionsYield
With dmap In dichloromethane at 0 - 30℃; for 19h;99%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

(1R,2R,4S)-1,7,7-trimethylbicyclo[2.2.1]hexane-2-ol

(1R,2R,4S)-1,7,7-trimethylbicyclo[2.2.1]hexane-2-ol

isobornyl acrylate

isobornyl acrylate

Conditions
ConditionsYield
With sulfuric acid In toluene at 60 - 80℃; for 4.5h; Solvent;98.9%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

tert-butyl (5R)-5-[[7-(3-hydroxy-1-naphthyl)-4-piperazin-1-yl-6,8-dihydro-5H-pyrido[3,4-d]pyrimidin-2-yl]oxymethyl]-2,2-dimethylpyrrolidine-1-carboxylate

tert-butyl (5R)-5-[[7-(3-hydroxy-1-naphthyl)-4-piperazin-1-yl-6,8-dihydro-5H-pyrido[3,4-d]pyrimidin-2-yl]oxymethyl]-2,2-dimethylpyrrolidine-1-carboxylate

tert-butyl (5R)-5-[[7-(3-hydroxy-1-naphthyl)-4-(4-prop-2-enoylpiperazin-1-yl)-6,8-dihydro-5H-pyrido[3,4-d]pyrimidin-2-yl]oxymethyl]-2,2-dimethyl-pyrrolidine-1-carboxylate

tert-butyl (5R)-5-[[7-(3-hydroxy-1-naphthyl)-4-(4-prop-2-enoylpiperazin-1-yl)-6,8-dihydro-5H-pyrido[3,4-d]pyrimidin-2-yl]oxymethyl]-2,2-dimethyl-pyrrolidine-1-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at -40℃; for 1h; Inert atmosphere;98.6%
With N-ethyl-N,N-diisopropylamine In dichloromethane at -40℃; for 1h; Inert atmosphere;98.6%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

isobutylamine
78-81-9

isobutylamine

Propiolic acid
471-25-0

Propiolic acid

1-isobutyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxylic acid

1-isobutyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxylic acid

Conditions
ConditionsYield
Stage #1: acrylic acid anhydride; isobutylamine; Propiolic acid Solid phase reaction;
Stage #2: With 3percent TFA In dichloromethane at 20℃; for 2h; Hydrolysis; Further stages.;
98%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

isopropylamine
75-31-0

isopropylamine

Propiolic acid
471-25-0

Propiolic acid

1-isopropyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxylic acid

1-isopropyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxylic acid

Conditions
ConditionsYield
Stage #1: acrylic acid anhydride; isopropylamine; Propiolic acid Solid phase reaction;
Stage #2: With 3percent TFA In dichloromethane at 20℃; for 2h; Hydrolysis; Further stages.;
98%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

N-tert-butyloxycarbonyl-β-tert-butyl-L-aspartyl-D-alaninol

N-tert-butyloxycarbonyl-β-tert-butyl-L-aspartyl-D-alaninol

acrylic acid
79-10-7

acrylic acid

Conditions
ConditionsYield
In pyridine; ethyl acetate; benzene97.8%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

benzaldehyde
100-52-7

benzaldehyde

phenylmethylene diacrylate

phenylmethylene diacrylate

Conditions
ConditionsYield
With toluene-4-sulfonic acid at 20℃; for 12h;97%
With toluene-4-sulfonic acid at 20℃; for 12h;97%
With sulfuric acid; copper
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

1-adamanthanol
768-95-6

1-adamanthanol

1-acryloyloxy-adamantane
121601-93-2

1-acryloyloxy-adamantane

Conditions
ConditionsYield
Acidic catalyst In cyclohexane Heating;95%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

1,3-dimethyl-5-adamantanol
707-37-9

1,3-dimethyl-5-adamantanol

3,5-Dimethyl-1-adamantyl acrylate
23743-72-8

3,5-Dimethyl-1-adamantyl acrylate

Conditions
ConditionsYield
Acidic catalyst In cyclohexane Heating;95%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

isobutylamine
78-81-9

isobutylamine

Propiolic acid
471-25-0

Propiolic acid

1-isobutyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxamide

1-isobutyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxamide

Conditions
ConditionsYield
Stage #1: acrylic acid anhydride; isobutylamine; Propiolic acid Solid phase reaction;
Stage #2: With 3percent TFA In dichloromethane at 20℃; for 2h; Hydrolysis; Further stages.;
95%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

N-(fluoren-9-ylmethoxycarbonyl)glycine
29022-11-5

N-(fluoren-9-ylmethoxycarbonyl)glycine

ethyl acetoacetate
141-97-9

ethyl acetoacetate

ethyl 1-carbamoylmethyl-6-methyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxylate

ethyl 1-carbamoylmethyl-6-methyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxylate

Conditions
ConditionsYield
Stage #1: acrylic acid anhydride; N-(fluoren-9-ylmethoxycarbonyl)glycine; ethyl acetoacetate Solid phase reaction;
Stage #2: With 3percent TFA In dichloromethane at 20℃; for 2h; Hydrolysis; Further stages.;
95%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

isopropylamine
75-31-0

isopropylamine

Propiolic acid
471-25-0

Propiolic acid

1-isopropyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxamide

1-isopropyl-2-oxo-1,2,3,4-tetrahydro-5-pyridinecarboxamide

Conditions
ConditionsYield
Stage #1: acrylic acid anhydride; isopropylamine; Propiolic acid Solid phase reaction;
Stage #2: With 3percent TFA In dichloromethane at 20℃; for 2h; Hydrolysis; Further stages.;
95%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

2,4,6-triiodo-5-aminoisophthalic acid
35453-19-1

2,4,6-triiodo-5-aminoisophthalic acid

2,4,6-triiodo-5-(prop-2-enamido)benzene-1,3-dicarboxylic acid
783279-02-7

2,4,6-triiodo-5-(prop-2-enamido)benzene-1,3-dicarboxylic acid

Conditions
ConditionsYield
With sulfuric acid In acetonitrile at 80℃;95%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

spiro(fluorene-9,9′-xanthene)-3',6'-diol
4081-00-9

spiro(fluorene-9,9′-xanthene)-3',6'-diol

spiro[9H-fluorene-9,9'-xanthene]-3',6'-diacrylate

spiro[9H-fluorene-9,9'-xanthene]-3',6'-diacrylate

Conditions
ConditionsYield
Stage #1: spiro[fuoroline-9,9'-(2',7'-dihydroxyxanthone)] With dmap; triethylamine In dichloromethane at 0℃; for 0.5h;
Stage #2: acrylic acid anhydride In dichloromethane at 0℃; for 5h;
94.7%
morpholine
110-91-8

morpholine

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

N-Acryloylmorpholine
5117-12-4

N-Acryloylmorpholine

Conditions
ConditionsYield
With 10H-phenothiazine; sulfuric acid for 2h; Reagent/catalyst; Heating;93.12%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

N-(fluoren-9-ylmethoxycarbonyl)glycine
29022-11-5

N-(fluoren-9-ylmethoxycarbonyl)glycine

3,4-dihydronaphthalene-1(2H)-one
529-34-0

3,4-dihydronaphthalene-1(2H)-one

2-(3-oxo-1,2,3,4,5,6-hexahydrobenzo[f]quinolin-4-yl)acetamide

2-(3-oxo-1,2,3,4,5,6-hexahydrobenzo[f]quinolin-4-yl)acetamide

Conditions
ConditionsYield
Stage #1: acrylic acid anhydride; N-(fluoren-9-ylmethoxycarbonyl)glycine; 3,4-dihydronaphthalene-1(2H)-one Solid phase reaction;
Stage #2: With 3percent TFA In dichloromethane at 20℃; for 2h; Hydrolysis; Further stages.;
92%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

5,12-di-tert-pentyl-7,16-di-tert-butyl-8,15-diisopropyl-4,13-dihydroxy[2,2]paracyclophane

5,12-di-tert-pentyl-7,16-di-tert-butyl-8,15-diisopropyl-4,13-dihydroxy[2,2]paracyclophane

C43H66O3

C43H66O3

Conditions
ConditionsYield
With n-butyllithium In acetone at 15 - 60℃; for 2h; Inert atmosphere;91%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

(S)-4-Benzyl-2-oxazolidinone
90719-32-7

(S)-4-Benzyl-2-oxazolidinone

(S)-3-acryloyl-4-benzyloxazolidin-2-one
90719-27-0

(S)-3-acryloyl-4-benzyloxazolidin-2-one

Conditions
ConditionsYield
With lithium chloride In tetrahydrofuran at 20℃; for 8h;90%
With lithium chloride In tetrahydrofuran Ambient temperature; Yield given;
With lithium chloride In tetrahydrofuran at -20 - 20℃; for 24h;2.914 g
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

1-Morpholino-4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-2-undecanol
170659-85-5

1-Morpholino-4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-2-undecanol

1-Morpholinomethyl-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl acrylate

1-Morpholinomethyl-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl acrylate

Conditions
ConditionsYield
In dichloromethane for 5h; Heating;90%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

2,6-di-tert-butylphenol
128-39-2

2,6-di-tert-butylphenol

1-(3,5-di-tert-butyl-4-hydroxyphenyl)vinyl ketone

1-(3,5-di-tert-butyl-4-hydroxyphenyl)vinyl ketone

Conditions
ConditionsYield
With perchloric acid for 1h; Ambient temperature;90%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

C10H11NO5

C10H11NO5

C16H15NO7

C16H15NO7

Conditions
ConditionsYield
With dmap In methanol; chloroform at 50℃; for 1h; Inert atmosphere;89%
4-(4-(2-(difluoromethyl)-1H-benzo[d]imidazol-1-yl)-6-(piperazin-1-yl)-1,3,5-triazin-2-yl)morpholine

4-(4-(2-(difluoromethyl)-1H-benzo[d]imidazol-1-yl)-6-(piperazin-1-yl)-1,3,5-triazin-2-yl)morpholine

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

1-(4-(4-(2-(difluoromethyl)-1H-benzo[d]imidazol-1-yl)-6-morpholino-1,3,5-triazin-2-yl)piperazin-1-yl)prop-2-en-1-one
1345988-62-6

1-(4-(4-(2-(difluoromethyl)-1H-benzo[d]imidazol-1-yl)-6-morpholino-1,3,5-triazin-2-yl)piperazin-1-yl)prop-2-en-1-one

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h;88%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

(1S,2R)-2-tert-Butoxycarbonylamino-cyclohexylamine
364385-54-6

(1S,2R)-2-tert-Butoxycarbonylamino-cyclohexylamine

tert-butyl ((1R,2S)-2-acrylamidocyclohexyl)carbamate

tert-butyl ((1R,2S)-2-acrylamidocyclohexyl)carbamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h; Temperature; Concentration; Cooling with ice; Inert atmosphere;87%
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; Inert atmosphere;74%
Stage #1: acrylic acid anhydride; (1S,2R)-2-tert-Butoxycarbonylamino-cyclohexylamine With triethylamine In dichloromethane at 20℃; for 0.5h; Cooling with ice; Inert atmosphere;
Stage #2: With methanesulfonic acid In dichloromethane at 20℃; for 5h; Inert atmosphere;
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

2-(2-hydroxyethyl)-4-(hydroxymethyl)-3a,4,7,7a-tetrahydro-1H-4,7-epoxyisoindole-1,3(2H)-dione

2-(2-hydroxyethyl)-4-(hydroxymethyl)-3a,4,7,7a-tetrahydro-1H-4,7-epoxyisoindole-1,3(2H)-dione

C17H17NO7

C17H17NO7

Conditions
ConditionsYield
With pyridine In methanol; dichloromethane at 30℃; for 2.5h; Inert atmosphere;87%
acrylic acid anhydride
2051-76-5

acrylic acid anhydride

(1S,2R)-2-(N-t-butyloxycarbonylamino)-1-aminocyclopentane
721395-15-9

(1S,2R)-2-(N-t-butyloxycarbonylamino)-1-aminocyclopentane

tert-butyl ((1R,2S)-2-acrylamidocyclopentyl)carbamate

tert-butyl ((1R,2S)-2-acrylamidocyclopentyl)carbamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice; Inert atmosphere;87%
4-methyl-1,4-pentanediol
1462-10-8

4-methyl-1,4-pentanediol

acrylic acid anhydride
2051-76-5

acrylic acid anhydride

4-(4-methylpentane-1,4-diyl)diacrylate

4-(4-methylpentane-1,4-diyl)diacrylate

Conditions
ConditionsYield
With N,N,N,N,-tetramethylethylenediamine at 60℃;86%

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