2-METHOXYPROPIONIC ACID METHYL ESTER

Base Information

• Chemical Name: 2-METHOXYPROPIONIC ACID METHYL ESTER
• CAS No.: 92935-45-0
• Molecular Formula: C₅H₁₀O₃
• Molecular Weight: 118.133
• Mol file: 92935-45-0.mol

Synonyms:2-METHOXYPROPIONIC ACID METHYL ESTER

Chemical Property of 2-METHOXYPROPIONIC ACID METHYL ESTER

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-METHOXYPROPIONIC ACID METHYL ESTER

There total 34 articles about 2-METHOXYPROPIONIC ACID METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.7%

methanol (67-56-1) + methyl lactate (547-64-8,2155-30-8) → methyl 2-methoxypropionate (17639-76-8,92935-45-0)

Guidance literature:

5% by weight NaH2PO4/SiO2; at 260 ℃; for 60h; Product distribution / selectivity; Gas phase;

Reference yield: 90.0%

methanol (67-56-1) + LACTIC ACID (849585-22-4,106989-11-1,26811-96-1,31587-11-8,26100-51-6) + methyl lactate (547-64-8,2155-30-8) → methyl 2-methoxypropionate (17639-76-8,92935-45-0)

Guidance literature:

(0.1% CaHPO4 and 5% K2HPO4)/SiO2; at 300 ℃; for 60h; Product distribution / selectivity; Gas phase;

Reference yield: 50.1%

2-methyl-2,3-pentadiene (3043-33-2) → methyl 2-methoxypropionate (17639-76-8,92935-45-0) + methyl 2-methoxy-2-methylpropanoate (17860-39-8) + 2-Methoxy-4-methyl-4-penten-3-on (57745-55-8) + 2,4-Dimethoxy-2-methyl-pentan-3-one (75075-40-0) + 1,4-Dimethoxy-4-methyl-pentan-3-one (75075-41-1)

Guidance literature:

With lithium perchlorate; In methanol; at 10 ℃; Product distribution; Mechanism; other electrolyte, other electrode, various oxidation potentials, various electricity consumptions, various electrolyte concentrations examined;

DOI:10.1016/0040-4020(82)80146-4

upstream raw materials:

methanol

(2R)-methyl 2-bromopropionate

R-(+)-2-methoxypropionic acid chloride

Methyl 2-bromopropionate

Downstream raw materials:

(S)-4-Benzyloxy-3-hydroxy-2-methoxy-2-methyl-pentanoic acid methyl ester

methyl 4-O-benzyl-5-deoxy-2-C-methyl-2-O-methyl-L-xylonate

methyl 4-O-benzyl-5-deoxy-2-C-methyl-2-O-methyl-4-L-ribonate

methyl 4-O-benzyl-5-deoxy-2-C-methyl-2-O-methyl-4-L-lyxonate