3-(tert-butyl)-1-methyl-1H-pyrazole-5-carbonitrile

Base Information

Chemical Name:3-(tert-butyl)-1-methyl-1H-pyrazole-5-carbonitrile
CAS No.:1196104-01-4
Molecular Formula:C9H13N3
Molecular Weight:163.222
Hs Code.:2933199090
Mol file:1196104-01-4.mol

Synonyms:3-(tert-butyl)-1-methyl-1H-pyrazole-5-carbonitrile

Suppliers and Price of 3-(tert-butyl)-1-methyl-1H-pyrazole-5-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile 95.0%
5 g
$ 685.00

SynQuest Laboratories
5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile 95.0%
1 g
$ 184.00

Matrix Scientific
5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile 95%+
1g
$ 270.00

Matrix Scientific
5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile 95%+
5g
$ 990.00

Apolloscientific
5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile
5g
$ 578.00

Apolloscientific
5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile
1g
$ 156.00

Advanced Chemicals Intermediatesced Chemicals Intermediates
5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile 95%+
1g
$ 108.75

Acints
5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile 95%+
1g
$ 108.75

Total 2 raw suppliers

Chemical Property of 3-(tert-butyl)-1-methyl-1H-pyrazole-5-carbonitrile

Chemical Property:

PSA：41.61000
LogP:1.58928

Purity/Quality:

97% ^*data from raw suppliers

5-tert-Butyl-2-methyl-2H-pyrazole-3-carbonitrile 95.0% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(tert-butyl)-1-methyl-1H-pyrazole-5-carbonitrile

There total 1 articles about 3-(tert-butyl)-1-methyl-1H-pyrazole-5-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82560-12-1,1237537-54-0
3-tert-butyl-1H-pyrazole-5-amine

: 1196104-01-4
3-tert-butyl-1H-pyrazol-5-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h

1.2: 0.5 h / 75 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C

2.2: 0.5 h / 100 °C

With hydrogenchloride; sodium hydride; sodium nitrite; In water; N,N-dimethyl-formamide;

Reference yield:

: 1196104-01-4
3-tert-butyl-1H-pyrazol-5-carbonitrile

: 1196103-46-4
3-tert-butyl-5-{5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl]-1H-imidazol-2-yl}-1-methyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride; methanol / mineral oil / 2 h / 40 °C / Inert atmosphere

1.2: 16 h / 70 °C

2.1: isopropyl alcohol / 3 h / 70 °C

With methanol; sodium hydride; In isopropyl alcohol; mineral oil;

Reference yield:

: 1196104-01-4
3-tert-butyl-1H-pyrazol-5-carbonitrile

: 1196103-36-2
3-(5-tert-butyl-2-methyl-2H-pyrazol-3-yl)-5-[1-(4-chloro-benzenesulfonyl)-1-methyl-ethyl]-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride; methanol / mineral oil / 2 h / 40 °C / Inert atmosphere

1.2: 16 h / 70 °C

2.1: sodium methylate / methanol / 42 h / Reflux

With methanol; sodium methylate; sodium hydride; In methanol; mineral oil;