1,3-Dioxane-4,6-dione, 5-[[(3,4-diMethoxyphenyl)aMino]Methylene]-2,2-diMethyl-

Base Information

• Chemical Name: 1,3-Dioxane-4,6-dione, 5-[[(3,4-diMethoxyphenyl)aMino]Methylene]-2,2-diMethyl-
• CAS No.: 213699-53-7
• Molecular Formula: C15H17NO6
• Molecular Weight: 307.303
• Mol file: 213699-53-7.mol

Synonyms:1,3-Dioxane-4,6-dione, 5-[[(3,4-diMethoxyphenyl)aMino]Methylene]-2,2-diMethyl-

Chemical Property of 1,3-Dioxane-4,6-dione, 5-[[(3,4-diMethoxyphenyl)aMino]Methylene]-2,2-diMethyl-

Chemical Property:

• PSA: 83.09000
• LogP: 1.90870

Purity/Quality:

97% ^*data from raw suppliers

5-(((3,4-Dimethoxyphenyl)amino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-Dioxane-4,6-dione, 5-[[(3,4-diMethoxyphenyl)aMino]Methylene]-2,2-diMethyl-

There total 6 articles about 1,3-Dioxane-4,6-dione, 5-[[(3,4-diMethoxyphenyl)aMino]Methylene]-2,2-diMethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

cycl-isopropylidene malonate (2033-24-1) + orthoformic acid triethyl ester (122-51-0) + 3,4-dimethoxyaniline (6315-89-5) → 5-(((3,4-dimethoxyphenyl)amino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (213699-53-7)

Guidance literature:

In ethanol; at -20 ℃; Reflux;

Reference yield: 85.5%

cycl-isopropylidene malonate (2033-24-1) + 3,4-dimethoxyaniline (6315-89-5) → 5-(((3,4-dimethoxyphenyl)amino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (213699-53-7)

Guidance literature:

3,4-dimethoxyaniline; With orthoformic acid triethyl ester; at 20 ℃; for 0.5h;

cycl-isopropylidene malonate; at 90 ℃; for 3.5h;

Reference yield: 85.5%

CH(OC2H5)3 + 3,4-dimethoxyaniline (6315-89-5) → 5-(((3,4-dimethoxyphenyl)amino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (213699-53-7)

Guidance literature:

In cycl-isopropylidene malonate;

upstream raw materials:

5-methoxymethylene-2,2-dimethyl-1,3-dioxane-4,6-dione

3,4-dimethoxyaniline

cycl-isopropylidene malonate

orthoformic acid triethyl ester

Downstream raw materials:

6,7-dimethoxyquinoline-4-ol

5,6-dimethoxy-quinolin-4-ol

1,4-dihydro-6,7-dimethoxy-4-oxoquinoline

6,7-dimethoxy-4-chloroquinoline