2-methyl-2-(4-morpholinyl)-1-propanol(SALTDATA: FREE)

Base Information

• Chemical Name: 2-methyl-2-(4-morpholinyl)-1-propanol(SALTDATA: FREE)
• CAS No.: 858197-58-7
• Molecular Formula: C8H17NO2
• Molecular Weight: 159.228
• Hs Code.: 2934999090
• Mol file: 858197-58-7.mol

Synonyms:2-methyl-2-(4-morpholinyl)-1-propanol(SALTDATA: FREE);2-Methyl-2-morpholin-4-ylpropan-1-ol;2-Methyl-2-(4-morpholinyl)-1-propanol

Chemical Property of 2-methyl-2-(4-morpholinyl)-1-propanol(SALTDATA: FREE)

Chemical Property:

• Vapor Pressure: 0.00582mmHg at 25°C
• Boiling Point: 242.4°C at 760 mmHg
• Flash Point: 100.4°C
• PSA: 32.70000
• Density: 1.045g/cm³
• LogP: 0.02740

Purity/Quality:

98%min ^*data from raw suppliers

2-methyl-2-morpholin-4-ylpropan-1-ol ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 41

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-methyl-2-(4-morpholinyl)-1-propanol(SALTDATA: FREE)

There total 2 articles about 2-methyl-2-(4-morpholinyl)-1-propanol(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl α-methyl-2-morpholinopropionate (87439-17-6) → 2-methyl-2-(morpholin-4-yl)propan-1-ol (858197-58-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 25 ℃;

Reference yield:

2-Amino-2-methyl-1-propanol (124-68-5) + 3-oxa-1,5-dichloropentane (111-44-4) → 2-methyl-2-(morpholin-4-yl)propan-1-ol (858197-58-7)

Guidance literature:

With potassium carbonate; at 170 ℃;

DOI:10.1021/ja01256a065

Reference yield: 34.0%

2-methyl-2-(morpholin-4-yl)propan-1-ol (858197-58-7) + 6-[(2,3-difluoro-4-hydroxyphenyl)methyl]-9-hydroxy-5-methyl-7-oxo-N-[4-(trifluoromethyl)-2-[6-(trifluoromethyl)pyrimidin-4-yl]phenyl]-5,6-diazaspiro[3.5]non-8-ene-8-carboxamide → 6-[[2,3-difluoro-4-(2-methyl-1-morpholin-4-ylpropan-2-yl)oxyphenyl]methyl]-9-hydroxy-5-methyl-7-oxo-N-[4-(trifluoromethyl)-2-[6-(trifluoromethyl)pyrimidin-4-yl]phenyl]-5,6-diazaspiro[3.5]non-8-ene-8-carboxamide

Guidance literature:

With diamide; trimethylphosphane; In tetrahydrofuran; at 60 ℃; for 16h;

upstream raw materials:

2-Amino-2-methyl-1-propanol

3-oxa-1,5-dichloropentane

ethyl α-methyl-2-morpholinopropionate

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