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2-Amino-2-methyl-1-propanol
Cas No: 124-68-5
USD $ 1.0-1.0 / Metric Ton 1 Metric Ton 1.5 Metric Ton/Day Hangzhou Keyingchem Co.,Ltd Contact Supplier
2-Amino-2-methyl-1-propanol supplier in China
Cas No: 124-68-5
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality 2-Amino-2-Methyl-1-Propanol with high purity
Cas No: 124-68-5
No Data 1 Kilogram 30 Metric Ton/Month Simagchem Corporation Contact Supplier
High purity 124-68-5 2-AMINO-2-METHYL-1-PROPANOL
Cas No: 124-68-5
USD $ 100.0-500.0 / Gram 1 Gram 99999 Gram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
High Quality 99% 124-68-5 2-Amino-2-methyl-1-propanol Manufacturer
Cas No: 124-68-5
USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
Factory Supply 2-amino-2-methylpropanol
Cas No: 124-68-5
No Data 1 1 Ality Chemical Corporation Contact Supplier
4-amino-2-methyl-N-propyl-3-pyrazolecarboxamide
Cas No: 124-68-5
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
2-Amino-2-methyl-1-propanol
Cas No: 124-68-5
USD $ 1.0-1.0 / Kilogram 10 Kilogram 1000 Kilogram/Month Enke Pharma-tech Co.,Ltd. (Cangzhou, China ) Contact Supplier
124-68-5 2-Amino-2-methyl-1-propanol
Cas No: 124-68-5
USD $ 1000.0-1000.0 / Kilogram 1 Kilogram 1 Metric Ton/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier
2-Amino-2-methyl-1-propanolcas124-68-5
Cas No: 124-68-5
USD $ 1.0-2.0 / Metric Ton 1 Metric Ton 2 Metric Ton/Day Hubei Jusheng Technology Co., Ltd., Contact Supplier

124-68-5 Usage

Chemical Properties

white crystals or viscous liquid

Fire Hazard

Special Hazards of Combustion Products: Emits toxic fumes during fire conditions.

Health Hazard

Causes severe irritation. Inhalation may be fatal as a result of spasm, inflammation, and edema of laryns and bronchi, chemical pneumonitis, and pulmonary edema. Symptoms of exposure may include burning sensation, coughing, wheezing, laryngitis, shortness of breath, headache, nausea and vomiting.

General Description

A clear light colored liquid. Insoluble in water and about the same density as water. Flash point 172°F. Used to make other chemicals.

Hazard

Toxic by ingestion.

Air & Water Reactions

Insoluble in water.

Purification Methods

Purify it by distilling and fractional freezing. The hydrochloride has m 204o-206o. [Beilstein 4 III 783, 4 IV 1740.]

Reactivity Profile

2-Amino-2-methyl-1-propanol is an aminoalcohol. Amines are chemical bases. They neutralize acids to form salts plus water. These acid-base reactions are exothermic. The amount of heat that is evolved per mole of amine in a neutralization is largely independent of the strength of the amine as a base. Amines may be incompatible with isocyanates, halogenated organics, peroxides, phenols (acidic), epoxides, anhydrides, and acid halides. Flammable gaseous hydrogen is generated by amines in combination with strong reducing agents, such as hydrides.

Uses

Used for the preparation of buffer solutions, suitable for the determination of alkaline phosphatase

124-68-5 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A17814)  2-Amino-2-methyl-1-propanol, 95%, may cont. ca 5% water    124-68-5 100ml 194.0CNY Detail
Alfa Aesar (A17814)  2-Amino-2-methyl-1-propanol, 95%, may cont. ca 5% water    124-68-5 500ml 249.0CNY Detail
Alfa Aesar (A17814)  2-Amino-2-methyl-1-propanol, 95%, may cont. ca 5% water    124-68-5 2500ml 989.0CNY Detail
Aldrich (A65182)  2-Amino-2-methyl-1-propanol  ~5% Water, technical grade, 90% 124-68-5 A65182-25ML 151.34CNY Detail
Aldrich (A65182)  2-Amino-2-methyl-1-propanol  ~5% Water, technical grade, 90% 124-68-5 A65182-500ML 224.64CNY Detail
Aldrich (A65182)  2-Amino-2-methyl-1-propanol  ~5% Water, technical grade, 90% 124-68-5 A65182-1L 443.43CNY Detail
Aldrich (A65182)  2-Amino-2-methyl-1-propanol  ~5% Water, technical grade, 90% 124-68-5 A65182-2.5L 716.04CNY Detail
Sigma-Aldrich (08581)  2-Amino-2-methyl-1-propanol  technical, ≥90% (GC) 124-68-5 08581-250ML 345.15CNY Detail
Sigma-Aldrich (08581)  2-Amino-2-methyl-1-propanol  technical, ≥90% (GC) 124-68-5 08581-1L 781.56CNY Detail

124-68-5SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-Amino-2-methyl-1-propanol

1.2 Other means of identification

Product number -
Other names 2-amino-2-methylpropan-1-ol

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Fillers,Intermediates,Lubricants and lubricant additives,Solvents (which become part of product formulation or mixture)
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:124-68-5 SDS

124-68-5Synthetic route

C13H17NO3

C13H17NO3

A

salicylaldehyde
90-02-8

salicylaldehyde

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With hydrogenchloride In water at 80℃; for 4h;A 96%
B 80%
carbon monoxide
201230-82-2

carbon monoxide

isopropylamine
75-31-0

isopropylamine

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With tricresyl phosphate; hydrogen; palladium diacetate In diphenylether at 140℃; under 22502.3 - 60006 Torr; Autoclave;93%
2,2-dimethylaziridine
2658-24-4

2,2-dimethylaziridine

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With sulfuric acid In water at 40 - 50℃; for 1h; pH=3 - 5.4;91%
2-(ethylamino)-2-methylpropanol hydrochloride
82922-13-2

2-(ethylamino)-2-methylpropanol hydrochloride

A

formaldehyd
50-00-0

formaldehyd

B

ethylamine
75-04-7

ethylamine

C

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

D

acetaldehyde
75-07-0

acetaldehyde

E

acetone
67-64-1

acetone

Conditions
ConditionsYield
With water at 25℃; Product distribution; Mechanism; anodic oxidation, carbonate buffer, pH 10; effect of substituents investigated with different types of β-alkanolamines;A 50%
B 44%
C 14%
D 26%
E 66%
2-(ethylamino)-2-methylpropanol hydrochloride
82922-13-2

2-(ethylamino)-2-methylpropanol hydrochloride

A

formaldehyd
50-00-0

formaldehyd

B

ethylamine
75-04-7

ethylamine

C

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

D

acetone
67-64-1

acetone

Conditions
ConditionsYield
With water at 25℃; anodic oxidation, pH 10, carbonate buffer; Further byproducts given;A 50%
B 44%
C 14%
D 66%
2-nitro-2-methylpropanol
76-39-1

2-nitro-2-methylpropanol

A

N-(1-hydroxy-2-methylprop-2-yl)-hydroxylamine
4706-13-2

N-(1-hydroxy-2-methylprop-2-yl)-hydroxylamine

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With citrate buffer; potassium chloride In ethanol at 30℃; cotrolled potential electrolysis, cathod: Hg, vs. S.C.E.;A 64%
B 25%
2-methyl-3-(vinyloxy)propan-2-amine
86241-96-5

2-methyl-3-(vinyloxy)propan-2-amine

A

N-ethylidene-2-methyl-1-vinyloxypropan-2-amine

N-ethylidene-2-methyl-1-vinyloxypropan-2-amine

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With mercury(II) diacetate In benzene Heating;A 3%
B n/a
2-nitro-2-methylpropanol
76-39-1

2-nitro-2-methylpropanol

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With methanol; carbon dioxide; nickel at 70℃; under 25742.8 Torr; Hydrogenation;
With methanol; nickel at 30℃; under 25742.8 Torr; Hydrogenation;
With nickel Hydrogenation;
2-methylalanine ethyl ester
1113-49-1

2-methylalanine ethyl ester

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With ethanol; nickel at 100℃; under 257428 Torr; Hydrogenation;
2-Aminoisobutyric acid
62-57-7

2-Aminoisobutyric acid

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With tetrahydrofuran; lithium aluminium tetrahydride
With lithium aluminium tetrahydride In tetrahydrofuran
With sodium tetrahydroborate; iodine In tetrahydrofuran for 20h; Heating;
With sodium tetrahydroborate; iodine In tetrahydrofuran Reflux;
With lithium aluminium tetrahydride In tetrahydrofuran
isobutene
115-11-7

isobutene

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
(i) MeCN, Cl2, (ii) H2O; Multistep reaction;
2-ammonio-2-methyl-1-propanol cation
22451-34-9

2-ammonio-2-methyl-1-propanol cation

C14H13NO
114444-46-1

C14H13NO

A

1-methyl-4-(phenylacetyl)pyridinium cation
124225-44-1

1-methyl-4-(phenylacetyl)pyridinium cation

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
In water at 25℃; Equilibrium constant; Rate constant;
N-chloro-2-amino-2-methylpropan-1-ol
116221-74-0

N-chloro-2-amino-2-methylpropan-1-ol

A

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

B

N,N-dichloro-2-amino-2-methyl-1-propanol

N,N-dichloro-2-amino-2-methyl-1-propanol

Conditions
ConditionsYield
In water at 25℃; Rate constant; Thermodynamic data; E(a);
3-Amino-1-(4,4-dimethyl-4,5-dihydro-oxazol-2-yl)-5-methyl-hexan-2-ol

3-Amino-1-(4,4-dimethyl-4,5-dihydro-oxazol-2-yl)-5-methyl-hexan-2-ol

A

statine
49642-07-1

statine

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

C

(3S,4R)-4-amino-3-hydroxy-6-methylheptanoic acid

(3S,4R)-4-amino-3-hydroxy-6-methylheptanoic acid

Conditions
ConditionsYield
With hydrogenchloride for 1h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
3-(N-succinimido)-2-propanol
87730-42-5

3-(N-succinimido)-2-propanol

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With hydrogenchloride; sodium tetrahydroborate In isopropyl alcohol
ethanol
64-17-5

ethanol

2-methylalanine ethyl ester
1113-49-1

2-methylalanine ethyl ester

Raney nickel

Raney nickel

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
at 100℃; under 250073 Torr; Hydrogenation;
2-amino-2-methylpropionic acid methyl ester
13257-67-5

2-amino-2-methylpropionic acid methyl ester

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With hydrogen; Nishimura catalyst <(45.9% Rh/19.9% Pt) oxide> In methanol at 25℃; under 75007.5 Torr;
methyl 2-aminoisobutyrate hydrochloride
15028-41-8

methyl 2-aminoisobutyrate hydrochloride

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With sodium tetrahydroborate; sodium hydrogencarbonate
2-((tert-butyloxycarbonyl)amino)-2-methylpropan-1-ol
102520-97-8

2-((tert-butyloxycarbonyl)amino)-2-methylpropan-1-ol

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane
trans-N-{4-[5-(2-Hydroxy-1,1-dimethyl-ethylamino)-pentyl]-cyclohexyl}-N-methyl-4-trifluoromethyl-benzenesulfonamide

trans-N-{4-[5-(2-Hydroxy-1,1-dimethyl-ethylamino)-pentyl]-cyclohexyl}-N-methyl-4-trifluoromethyl-benzenesulfonamide

A

trans-N-[4-(5-Bromo-pentyl)-cyclohexyl]-N-methyl-4-trifluoromethyl-benzenesulfonamide

trans-N-[4-(5-Bromo-pentyl)-cyclohexyl]-N-methyl-4-trifluoromethyl-benzenesulfonamide

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

(+)-pinanediol (1R)-1-acetylamino-1-[3-(4,4-dimethyl-4,5-dihydro-oxazol-2-yl)phenyl]methylboronate
497258-63-6

(+)-pinanediol (1R)-1-acetylamino-1-[3-(4,4-dimethyl-4,5-dihydro-oxazol-2-yl)phenyl]methylboronate

A

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

B

(1R)-1-acetylamino-1-(3-carboxyphenyl)methylboronic acid

(1R)-1-acetylamino-1-(3-carboxyphenyl)methylboronic acid

Conditions
ConditionsYield
With hydrogenchloride In water at 120℃; for 1h;
(2-hydroxy-1,1-dimethyl-ethyl)-carbamic acid

(2-hydroxy-1,1-dimethyl-ethyl)-carbamic acid

A

carbon dioxide
124-38-9

carbon dioxide

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
at 125℃; Inert atmosphere; Schlenk technique;
N-(1-hydroxy-2-methylpropan-2-yl)-1-naphthamide
117052-89-8

N-(1-hydroxy-2-methylpropan-2-yl)-1-naphthamide

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With sodium hydroxide In ethanol at 135℃; for 0.166667h; Microwave irradiation;
2-(hydroxymethyl)-2-methylpropylamine
32831-43-9

2-(hydroxymethyl)-2-methylpropylamine

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With sodium hypochlorite; sodium hydroxide In water at 0 - 70℃; for 0.333333h; Temperature; Hofmann Rearrangement;103 g
2-((E)-(1-hydroxy-2-methylpropan-2-ylimino)methyl)-6-methoxyphenol

2-((E)-(1-hydroxy-2-methylpropan-2-ylimino)methyl)-6-methoxyphenol

A

3-methoxy-2-hydroxybenzaldehyde
148-53-8

3-methoxy-2-hydroxybenzaldehyde

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With cerium(III) nitrate hexahydrate In methanol
N-(1-cyano-1-methyl-ethyl)formamide
58004-55-0

N-(1-cyano-1-methyl-ethyl)formamide

A

N-(1-hydroxy-2-methylpropan-2-yl)formamide
682-85-9

N-(1-hydroxy-2-methylpropan-2-yl)formamide

B

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); hydrogen In 1,4-dioxane; water at 140℃; under 33753.4 Torr; for 18h; Reagent/catalyst; Pressure; Autoclave;A n/a
B 24 %Spectr.
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); hydrogen In 1,4-dioxane; water at 20 - 150℃; under 41254.1 - 101260 Torr; for 48h; Autoclave;A n/a
B 73 %Chromat.
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); water; hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In 1,4-dioxane at 150℃; under 41254.1 - 101260 Torr; for 48h; Catalytic behavior; Pressure; Reagent/catalyst; Temperature; Autoclave;A 22 %Chromat.
B 58.3 %Chromat.
C13H17NO3

C13H17NO3

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With hydrogenchloride In water at 80℃;
N-(1-cyano-1-methyl-ethyl)formamide
58004-55-0

N-(1-cyano-1-methyl-ethyl)formamide

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Conditions
ConditionsYield
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; water; hydrogen; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 140℃; under 41254.1 Torr; for 18h; Catalytic behavior; Reagent/catalyst; Pressure; Autoclave;24 %Spectr.
2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2-amino-2-methylpropyl hydrogensulfate
927-82-2

2-amino-2-methylpropyl hydrogensulfate

Conditions
ConditionsYield
With sulfuric acid In water at 50 - 120℃; for 3h; Product distribution / selectivity;100%
With chlorosulfonic acid In diethyl ether at 0℃;96%
With sulfuric acid In water at 150 - 170℃; for 4h;94%
pyridine-2-carbaldehyde
1121-60-4

pyridine-2-carbaldehyde

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

4,4-dimethyl-2-pyridin-2-yl-1,3-oxazolidine
134777-99-4

4,4-dimethyl-2-pyridin-2-yl-1,3-oxazolidine

Conditions
ConditionsYield
In ethanol for 2h; Ambient temperature;100%
In ethanol at 20℃; for 3h;94%
pyridine-4-carbaldehyde
872-85-5

pyridine-4-carbaldehyde

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

4-(4,4-Dimethyl-oxazolidin-2-yl)-pyridine
134778-11-3

4-(4,4-Dimethyl-oxazolidin-2-yl)-pyridine

Conditions
ConditionsYield
In ethanol for 2h; Ambient temperature;100%
3-pyridinecarboxaldehyde
500-22-1

3-pyridinecarboxaldehyde

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

3-(4,4-Dimethyl-oxazolidin-2-yl)-pyridine
134778-05-5

3-(4,4-Dimethyl-oxazolidin-2-yl)-pyridine

Conditions
ConditionsYield
In ethanol for 2h; Ambient temperature;100%
benzoic acid ethyl ester
93-89-0

benzoic acid ethyl ester

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

N-(2-hydroxyl-1,1-dimethylethyl) benzamide
19312-05-1

N-(2-hydroxyl-1,1-dimethylethyl) benzamide

Conditions
ConditionsYield
Stage #1: 2-Amino-2-methyl-1-propanol With n-butyllithium; lanthanum(III) chloride In 1,2-dichloro-ethane at 0℃; Metallation; after the reagent addition stirring for 15 min at this temperature under nitrogen, than warming to reflux;
Stage #2: benzoic acid ethyl ester for 1h; Amidation; reflux;
100%
With sodium hydride 1.) toluene, RT, 1 h, 2.) toluene, 30 min; Yield given. Multistep reaction;
With n-butyllithium; lanthanum(lll) triflate 1) toluene, 0 deg C, 15 min then 0 to 100 deg C, 2) toluene, reflux, 12 h; Yield given. Multistep reaction;
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2-((tert-butyloxycarbonyl)amino)-2-methylpropan-1-ol
102520-97-8

2-((tert-butyloxycarbonyl)amino)-2-methylpropan-1-ol

Conditions
ConditionsYield
In acetonitrile at 20℃; Condensation;100%
With triethylamine In dichloromethane at 20℃; for 2.83333h;100%
Stage #1: di-tert-butyl dicarbonate With molybdenium(VI) dioxodichloride In dichloromethane at 20℃; for 0.5h;
Stage #2: 2-Amino-2-methyl-1-propanol In dichloromethane at 20℃; for 10h;
99%
5-methoxy-3-methylbenzoic acid chloride
96227-40-6

5-methoxy-3-methylbenzoic acid chloride

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

N-(2-Hydroxy-1,1-dimethyl-ethyl)-3-methoxy-5-methyl-benzamide

N-(2-Hydroxy-1,1-dimethyl-ethyl)-3-methoxy-5-methyl-benzamide

Conditions
ConditionsYield
In dichloromethane at 25℃; for 24h;100%
2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

N-(1-hydroxy-2-methylpropan-2-yl)-2-methylbenzamide
95217-40-6

N-(1-hydroxy-2-methylpropan-2-yl)-2-methylbenzamide

Conditions
ConditionsYield
In dichloromethane at 0℃; for 0.5h;100%
With triethylamine In dichloromethane at 0℃;
With triethylamine In dichloromethane at 0℃; for 3h; Inert atmosphere;
4-heptanone
123-19-3

4-heptanone

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

4,4-dimethyl-2,2-dipropyloxazolidine

4,4-dimethyl-2,2-dipropyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
n-pentyl methyl ketone
110-43-0

n-pentyl methyl ketone

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2,4,4-trimethyl-2-pentyloxazolidine
51805-99-3

2,4,4-trimethyl-2-pentyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
5-Nonanone
502-56-7

5-Nonanone

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2,2-dibutyl-4,4-dimethyloxazolidine
174153-08-3

2,2-dibutyl-4,4-dimethyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
2-Nonanone
821-55-6

2-Nonanone

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2-heptyl-2,4,4-trimethyloxazolidine

2-heptyl-2,4,4-trimethyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
Decan-2-one
693-54-9

Decan-2-one

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2,4,4-trimethyl-2-octyloxazolidine

2,4,4-trimethyl-2-octyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
dipentyl ketone
927-49-1

dipentyl ketone

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

4,4-dimethyl-2,2-dipentyloxazolidine
174153-09-4

4,4-dimethyl-2,2-dipentyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
methyl nonyl ketone
112-12-9

methyl nonyl ketone

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2,4,4-trimethyl-2-nonyloxazolidine
69184-35-6

2,4,4-trimethyl-2-nonyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
10-Nonadecanon
504-57-4

10-Nonadecanon

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

4,4-dimethyl-2,2-dinonyloxazolidine
174153-10-7

4,4-dimethyl-2,2-dinonyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

hexyl-methyl-ketone
111-13-7

hexyl-methyl-ketone

2-hexyl-2,4,4-trimethyloxazolidine

2-hexyl-2,4,4-trimethyloxazolidine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene Heating;100%
2,3-dimethoxyterephthalic acid chloride
7169-12-2

2,3-dimethoxyterephthalic acid chloride

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

N,N'-bis(2-hydroxy-1,1-dimethylethyl)-2,3-dimethoxyterephthalamide
179693-92-6

N,N'-bis(2-hydroxy-1,1-dimethylethyl)-2,3-dimethoxyterephthalamide

Conditions
ConditionsYield
In dichloromethane at 20℃; for 2h;100%
In dichloromethane; water6.27 g (100%)
2,3-bis(benzyloxy)benzoyl chloride
69146-58-3

2,3-bis(benzyloxy)benzoyl chloride

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2,3-dibenzyloxy-N-(2-hydroxy-1,1-dimethylethyl)benzamide
437613-96-2

2,3-dibenzyloxy-N-(2-hydroxy-1,1-dimethylethyl)benzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane for 6.5h;100%
2-hydroxy-3-phenylbenzaldehyde
14562-10-8

2-hydroxy-3-phenylbenzaldehyde

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

3-[(2-hydroxy-1,1-dimethylethylimino)methyl]biphenyl-2-ol

3-[(2-hydroxy-1,1-dimethylethylimino)methyl]biphenyl-2-ol

Conditions
ConditionsYield
for 1h; Heating;100%
2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2,2'-dihydroxybiphenyl-3-carboxaldehyde
156660-22-9

2,2'-dihydroxybiphenyl-3-carboxaldehyde

3-[(2-hydroxy-1,1-dimethylethylimino)methyl]biphenyl-2,2'-diol

3-[(2-hydroxy-1,1-dimethylethylimino)methyl]biphenyl-2,2'-diol

Conditions
ConditionsYield
for 1h; Heating;100%
acetic anhydride
108-24-7

acetic anhydride

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

N-(1-hydroxy-2-methylpropan-2-yl)acetamide
1569-96-6

N-(1-hydroxy-2-methylpropan-2-yl)acetamide

Conditions
ConditionsYield
Stage #1: acetic anhydride With molybdenium(VI) dioxodichloride In dichloromethane at 20℃; for 0.5h;
Stage #2: 2-Amino-2-methyl-1-propanol In dichloromethane at 20℃; for 0.5h;
100%
Stage #1: acetic anhydride; 2-Amino-2-methyl-1-propanol In ethyl acetate at 20℃; for 18h; Inert atmosphere;
Stage #2: With potassium carbonate In ethyl acetate at 20℃; Inert atmosphere; chemoselective reaction;
98%
With Methylenediphosphonic acid at 20℃; for 1h; neat (no solvent); chemoselective reaction;95%
With sodium hydrogencarbonate In water at 20℃; for 16h;
With triethylamine In chloroform at 20℃; for 24h; Temperature; chemoselective reaction;99 %Spectr.
2,2-dimethylpropanoic anhydride
1538-75-6

2,2-dimethylpropanoic anhydride

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

N-(2-hydroxy-1,1-dimethylethyl)-2,2-dimethylpropionamide
848598-54-9

N-(2-hydroxy-1,1-dimethylethyl)-2,2-dimethylpropionamide

Conditions
ConditionsYield
Stage #1: 2,2-dimethylpropanoic anhydride With molybdenium(VI) dioxodichloride In dichloromethane at 20℃; for 0.5h;
Stage #2: 2-Amino-2-methyl-1-propanol In dichloromethane at 20℃; for 1h;
100%
benzoyl chloride
98-88-4

benzoyl chloride

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

4,5-dihydro-4,4-dimethyl-2-phenoxazole
19312-06-2

4,5-dihydro-4,4-dimethyl-2-phenoxazole

Conditions
ConditionsYield
Stage #1: benzoyl chloride; 2-Amino-2-methyl-1-propanol In dichloromethane at 20℃; for 18h;
Stage #2: With thionyl chloride In dichloromethane Further stages.;
100%
Stage #1: benzoyl chloride; 2-Amino-2-methyl-1-propanol With triethylamine In dichloromethane at 0 - 20℃; for 10h;
Stage #2: With thionyl chloride In chloroform at 0 - 20℃; for 24h;
Stage #3: With sodium hydroxide In methanol at 0 - 20℃; for 12h;
92%
3-methyl-4-isocyanato-benzoic acid methyl ester
864296-43-5

3-methyl-4-isocyanato-benzoic acid methyl ester

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

4-(3-[1,1-dimethyl-2-hydroxy-ethyl]-ureido)-3-methyl-benzoic acid methyl ester
864296-97-9

4-(3-[1,1-dimethyl-2-hydroxy-ethyl]-ureido)-3-methyl-benzoic acid methyl ester

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 2h;100%
In tetrahydrofuran at 20℃; for 2h;
1-[[[(2,5-dioxopyrrolidin-1-yl)oxy]carbonyl]oxy]ethyl 2-methylpropanoate
860035-10-5

1-[[[(2,5-dioxopyrrolidin-1-yl)oxy]carbonyl]oxy]ethyl 2-methylpropanoate

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

[N-(2-hydroxy-tert-butyl)carbamoyloxy]ethyl 2-methylpropanoate
1131570-15-4

[N-(2-hydroxy-tert-butyl)carbamoyloxy]ethyl 2-methylpropanoate

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; acetonitrile at 20℃; for 12h;100%
2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

Diethyl methylmalonate
609-08-5

Diethyl methylmalonate

N,N'-bis(1-hydroxy-2-methylpropan-2-yl)-2-methylmalonamide

N,N'-bis(1-hydroxy-2-methylpropan-2-yl)-2-methylmalonamide

Conditions
ConditionsYield
With sodium hydride In mineral oil at 160℃; Inert atmosphere;100%
With sodium hydride at 140℃; for 4h; Inert atmosphere;95%
2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

diethyl 2-phenylmalonate
83-13-6

diethyl 2-phenylmalonate

N,N'-bis(1-hydroxy-2-methylpropan-2-yl)-2-phenylmalonamide

N,N'-bis(1-hydroxy-2-methylpropan-2-yl)-2-phenylmalonamide

Conditions
ConditionsYield
With sodium hydride In mineral oil at 160℃; Inert atmosphere;100%
2-tert-butylmalonyl dichloride
78775-72-1

2-tert-butylmalonyl dichloride

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2-tert-butyl-N,N'-bis(1-hydroxy-2-methylpropan-2-yl)malonamide

2-tert-butyl-N,N'-bis(1-hydroxy-2-methylpropan-2-yl)malonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere;100%
2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

diethyl malonate
105-53-3

diethyl malonate

N,N'-bis(1-hydroxy-2-methylpropan-2-yl)malonamide

N,N'-bis(1-hydroxy-2-methylpropan-2-yl)malonamide

Conditions
ConditionsYield
With sodium hydride In mineral oil at 160℃; Inert atmosphere;100%

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Carbon dioxide capture from pulp mill using 2-Amino-2-methyl-1-propanol (cas 124-68-5) and monoethanolamine blend: Techno-economic assessment of advanced process configuration09/25/2019

This project study involves the techno-economic assessment of two new advanced configurations for amine-based carbon dioxide capture from a pulp mill. The newly proposed advanced configurations include advanced rich amine four split (ARA4S), and advanced rich amine three split with desorber inte...detailed

Effect of ammonia on the kinetics of sulfur dioxide absorption into aqueous 2-Amino-2-methyl-1-propanol (cas 124-68-5) solutions09/24/2019

Rate constants for the reaction of aqueous 2-amino-2-methyl-1-propanol (AMP)/ammonia (NH3) solutions with SO2 were determined by measuring their SO2 absorption rates. The SO2 absorption characteristics of 30 wt% AMP solutions with added NH3(1, 3, and 5 wt%) were investigated using a stirred-cell...detailed

Mass transfer characteristics of CO2 absorption into 2-Amino-2-methyl-1-propanol (cas 124-68-5) non-aqueous solution in a microchannel09/09/2019

The gas–liquid two-phase flow and mass transfer performance of CO2 absorption into 2-amino-2-methyl-1-propanol (AMP) with ethylene glycol (EG) non-aqueous solution in a microchannel were investigated under different gas–liquid two-phase flow rates and AMP concentrations. A new correlation was ...detailed

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