[4R,(-)]-1,2,3,4,4aα,5,8,8aβ-Octahydro-6-methyl-1-methylene-4-isopropylnaphthalene

Base Information

Chemical Name:[4R,(-)]-1,2,3,4,4aα,5,8,8aβ-Octahydro-6-methyl-1-methylene-4-isopropylnaphthalene
CAS No.:5957-56-2
Molecular Formula:C₁₅H₂₄
Molecular Weight:204.356
Hs Code.:
Mol file:5957-56-2.mol

Synonyms:[4R,(-)]-1,2,3,4,4aα,5,8,8aβ-Octahydro-6-methyl-1-methylene-4-isopropylnaphthalene;3,10(15)-Cadinadiene;γ2-Cadinene

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Chemical Property of [4R,(-)]-1,2,3,4,4aα,5,8,8aβ-Octahydro-6-methyl-1-methylene-4-isopropylnaphthalene

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Technology Process of [4R,(-)]-1,2,3,4,4aα,5,8,8aβ-Octahydro-6-methyl-1-methylene-4-isopropylnaphthalene

There total 15 articles about [4R,(-)]-1,2,3,4,4aα,5,8,8aβ-Octahydro-6-methyl-1-methylene-4-isopropylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 81373-90-2
8-isopropyl-2-mesyloxymethyl-5-methylene-Δ²-decalene

: 5957-56-2,7089-89-6,29336-47-8,82166-09-4,122332-52-9
(+/-)-γ₂-cadinene

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; 1) overnight, 2) reflux, 3 h;

Reference yield: 39.0%

: 122305-06-0,122332-54-1
7-chloro-10-isopropyl-3,7-dimethylbicyclo<4.4.0>dec-3-ene

: 523-47-7,5951-61-1,6013-64-5,16509-53-8,122332-53-0,132296-09-4,5743-03-3
rac β-muurolene

: 5957-56-2,7089-89-6,29336-47-8,82166-09-4,122332-52-9
rac γ₂-muurolene

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; for 50h; Heating;
DOI:10.1016/S0040-4020(01)89792-1

Reference yield:

: 122305-05-9
trans-3-(4-chloro-2-methyl-2(E)-butenyl)-4-isopropyl-1-methylcyclohex-1-ene

: 5957-56-2,7089-89-6,29336-47-8,82166-09-4,122332-52-9
rac γ₂-muurolene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / ZnCl₂*Et₂O / CH₂Cl₂ / 25 h / -78 °C

2: 39 percent / potassium tert-butoxide / 2-methyl-propan-2-ol / 50 h / Heating

With potassium tert-butylate; zinc chloride diethyl ether; In dichloromethane; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)89792-1