2-Azabicyclo[2.2.1]hept-5-ene-3-carboxylicacid,ethylester,endo-(9CI)

Base Information

Chemical Name:2-Azabicyclo[2.2.1]hept-5-ene-3-carboxylicacid,ethylester,endo-(9CI)
CAS No.:166735-47-3
Molecular Formula:C₉H₁₃NO₂
Molecular Weight:167.208
Hs Code.:
Mol file:166735-47-3.mol

Synonyms:2-Azabicyclo[2.2.1]hept-5-ene-3-carboxylicacid,ethylester,endo-(9CI)

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Chemical Property of 2-Azabicyclo[2.2.1]hept-5-ene-3-carboxylicacid,ethylester,endo-(9CI)

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Technology Process of 2-Azabicyclo[2.2.1]hept-5-ene-3-carboxylicacid,ethylester,endo-(9CI)

There total 10 articles about 2-Azabicyclo[2.2.1]hept-5-ene-3-carboxylicacid,ethylester,endo-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: ethyl (1R,3S,4S)-2-[(1R)-1-phenylethyl]-2-azabicyclo[2.2.1]hept-5-ene-3-carboxylate

: 166735-47-3
2-tert-butyl 3-ethyl-2-azabicyclo[2.2.1]hept-5-ene-2,3-dicarboxylate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; ethyl acetate; for 23h; under 2585.81 Torr;

Reference yield: 98.0%

: 223505-12-2
(1R,3R,4S)-2-<(1S)-phenylethyl>-2-aza-bicyclo<2.2.1>hept-5-ene-3-carboxylic acid ethyl ester

: 166735-47-3
(1R,3R,4S)-2-Aza-bicyclo[2.2.1]hept-5-ene-3-carboxylic acid ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 48h; Ambient temperature;
DOI:10.1016/S0040-4020(98)00424-4

Reference yield: 90.0%

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 37662-05-8
((R)-1-phenyl-ethylimino)-acetic acid ethyl ester

: 764622-98-2,166735-47-3
(1S,3S,4R)-2-Aza-bicyclo[2.2.1]hept-5-ene-3-carboxylic acid ethyl ester

Guidance literature:: ((R)-1-phenyl-ethylimino)-acetic acid ethyl ester; With trifluoroacetic acid; In N,N-dimethyl-formamide; for 0.166667h;

cyclopenta-1,3-diene; In water; N,N-dimethyl-formamide; at 20 ℃; for 12h;