3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl

Base Information

Chemical Name:3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl
CAS No.:81998-07-4
Molecular Formula:C₁₂H₁₂N₂O
Molecular Weight:200.24
Hs Code.:
Mol file:81998-07-4.mol

Synonyms:3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl

Suppliers and Price of 3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl >98.0%(GC)(T)
200mg
$ 253.00

TCI Chemical
3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl >98.0%(GC)(T)
1g
$ 880.00

Crysdot
4,4'-Dimethyl-[2,2'-bipyridin]-3-ol 95+%
1g
$ 731.00

Chemenu
4,4''-Dimethyl-[2,2''-bipyridin]-3-ol 95%
1g
$ 690.00

Alichem
4,4'-Dimethyl-[2,2'-bipyridin]-3-ol
1g
$ 854.70

AK Scientific
3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl
200mg
$ 405.00

Total 6 raw suppliers

Chemical Property of 3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl

Chemical Property:

Melting Point:108.0 to 112.0 °C
PSA：46.01000
LogP:2.46600

Purity/Quality:

97% ^*data from raw suppliers

3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl >98.0%(GC)(T) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl

There total 2 articles about 3-Hydroxy-4,4'-dimethyl-2,2'-bipyridyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1134-35-6
4,4'-dimethyl-2,2'-bipyridines

: 81998-07-4
4,4'-dimethyl-3-hydroxy-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / 3-chloroperoxybenzoic acid / CHCl₃ / 48 h / Ambient temperature

2: 1.) acetic anhydride, 2.) 10percent aq. NaOH / 1.) 60-65 deg C, 24 h, 2.) aq. EtOH, reflux, 30 min

With sodium hydroxide; acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1021/jo00268a042

Reference yield:

: 81998-03-0
4,4’-dimethyl-2,2’-bipyridine N-oxide

: 118724-28-0
4,4'-dimethyl-5-hydroxy-2,2'-bipyridine

: 81998-04-1
4-(hydroxymethyl)-4'-methyl-2,2'-bipyridine

: 81998-07-4
4,4'-dimethyl-3-hydroxy-2,2'-bipyridine

Guidance literature:: With sodium hydroxide; acetic anhydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) 60-65 deg C, 24 h, 2.) aq. EtOH, reflux, 30 min;
DOI:10.1021/jo00268a042