2,3,4-TRI-O-ACETYL-D-XYLOPYRANOSE

Base Information

• Chemical Name: 2,3,4-TRI-O-ACETYL-D-XYLOPYRANOSE
• CAS No.: 55018-54-7
• Molecular Formula: C₁₁H₁₆O₈
• Molecular Weight: 276.243
• Mol file: 55018-54-7.mol

Synonyms:2,3,4-TRI-O-ACETYL-D-XYLOPYRANOSE;D-Xylose 2,3,4-Triacetate

Chemical Property of 2,3,4-TRI-O-ACETYL-D-XYLOPYRANOSE

Chemical Property:

• Storage Temp.: -20°C Freezer
• Solubility.: Chloroform, Ethyl Acetate, Methanol

Purity/Quality:

95% ^*data from raw suppliers

2,3,4-Tri-O-acetyl-D-xylopyranose ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,3,4-Tri-O-acetyl-D-xylopyranose is used in the synthesis of D-xylopyranose series: 2,3,4-Tri-O-acetyl-D-xylopyranose is used in the synthesis of D-xylopyranose series: tri-O-acetyl-D-xyloses and chloroacetyl derivatives.

Technology Process of 2,3,4-TRI-O-ACETYL-D-XYLOPYRANOSE

There total 4 articles about 2,3,4-TRI-O-ACETYL-D-XYLOPYRANOSE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-2,3,4-tri-O-acetyl-α-D-xylopyranose (3068-31-3) → O2,O3,O4-Triacetyl-D-xylose (55018-54-7)

Guidance literature:

With dimethyl sulfoxide; und anschliessend mit Chloroform und Wasser;

Reference yield:

2,3,4-tri-O-acetyl-α-L-xylopyranosyl bromide (65914-26-3) → O2,O3,O4-Triacetyl-L-xylose (55018-54-7,71024-10-7,85230-84-8,100924-40-1,107961-32-0)

Guidance literature:

With acetone; silver carbonate;

DOI:10.1021/ja01303a035

Reference yield:

1-bromo-2,3,4-tri-O-acetyl-α-D-xylopyranose (3068-31-3) + tert-butyl alcohol (75-65-0) → O2,O3,O4-Triacetyl-D-xylose (55018-54-7) + tert-butyl 2,3,4-tri-O-acetyl-β-D-xylopyranoside (6743-57-3)

Guidance literature:

With silver carbonate; benzene;

upstream raw materials:

2,3,4-tri-O-acetyl-α-L-xylopyranosyl bromide

1-bromo-2,3,4-tri-O-acetyl-α-D-xylopyranose

tert-butyl alcohol

iodine

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