Bis(2-nitrobenzyl) phosphorochloridate

Base Information

Chemical Name:Bis(2-nitrobenzyl) phosphorochloridate
CAS No.:56883-17-1
Molecular Formula:C14H12ClN2O7P
Molecular Weight:386.68
Hs Code.:
DSSTox Substance ID:DTXSID80391342
Wikidata:Q82188742

Synonyms:BIS(2-NITROBENZYL) PHOSPHOROCHLORIDATE;56883-17-1;DTXSID80391342;Bis(2-nitrobenzyl)phosphorochloridate;FT-0736128

Suppliers and Price of Bis(2-nitrobenzyl) phosphorochloridate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Bis(2-nitrobenzyl) phosphorochloridate

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:6
Exact Mass:386.0070654
Heavy Atom Count:25
Complexity:482

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)COP(=O)(OCC2=CC=CC=C2[N+](=O)[O-])Cl)[N+](=O)[O-]

Technology Process of Bis(2-nitrobenzyl) phosphorochloridate

There total 3 articles about Bis(2-nitrobenzyl) phosphorochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 56883-16-0
bis(2-nitrobenzyl) hydrogen phosphate

: 56883-17-1
di(2-nitrobenzyl) chlorophosphate

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ja200808y

Reference yield:

: 612-25-9
2-Nitrobenzyl alcohol

: 56883-17-1
di(2-nitrobenzyl) chlorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; phosphorodichloridic acid

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

With pyridine; oxalyl dichloride; phosphorodichloridic acid; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/ja200808y