Propanoic acid, 2,2-dimethyl-, octahydro-6,7,8-tris(methoxymethoxy)-1-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-

Base Information

Chemical Name:Propanoic acid, 2,2-dimethyl-, octahydro-6,7,8-tris(methoxymethoxy)-1-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-
CAS No.:156150-87-7
Molecular Formula:C₁₉H₃₅NO₈
Molecular Weight:405.489
Hs Code.:
Mol file:156150-87-7.mol

Synonyms:Propanoic acid, 2,2-dimethyl-, octahydro-6,7,8-tris(methoxymethoxy)-1-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanoic acid, 2,2-dimethyl-, octahydro-6,7,8-tris(methoxymethoxy)-1-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-

Chemical Property:

PSA：84.92000
LogP:0.93740

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Propanoic acid, 2,2-dimethyl-, octahydro-6,7,8-tris(methoxymethoxy)-1-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-

There total 1 articles about Propanoic acid, 2,2-dimethyl-, octahydro-6,7,8-tris(methoxymethoxy)-1-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13057-17-5
bromethyl methyl ether

: 156150-86-6
2,2-Dimethyl-propionic acid (1S,6S,7R,8R,8aS)-6,7,8-trihydroxy-octahydro-indolizin-1-yl ester

: 156150-87-7
2,2-Dimethyl-propionic acid (1S,6S,7R,8R,8aR)-6,7,8-tris-methoxymethoxy-octahydro-indolizin-1-yl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In toluene; at 90 ℃;
DOI:10.1016/S0040-4039(00)76852-3

Reference yield:

: 156150-87-7
2,2-Dimethyl-propionic acid (1S,6S,7R,8R,8aR)-6,7,8-tris-methoxymethoxy-octahydro-indolizin-1-yl ester

: 156150-85-5
2,2-Dimethyl-propionic acid (1S,6S,7S,8R,8aS)-6-(2,2-dimethyl-propionyloxy)-7,8-dihydroxy-octahydro-indolizin-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄

2: 1.) dibutyltin oxide / 1.) ref., toluene; 2.) -10 deg C

With lithium aluminium tetrahydride; di(n-butyl)tin oxide;
DOI:10.1016/S0040-4039(00)76852-3

Reference yield:

: 156150-87-7
2,2-Dimethyl-propionic acid (1S,6S,7R,8R,8aR)-6,7,8-tris-methoxymethoxy-octahydro-indolizin-1-yl ester

: 156150-86-6
2,2-Dimethyl-propionic acid (1S,6S,7R,8R,8aS)-6,7,8-trihydroxy-octahydro-indolizin-1-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄

2: 1.) dibutyltin oxide / 1.) ref., toluene; 2.) -10 deg C

3: KCN / methanol / Heating

With potassium cyanide; lithium aluminium tetrahydride; di(n-butyl)tin oxide; In methanol;
DOI:10.1016/S0040-4039(00)76852-3