5,6,7,8-Tetrahydro-2-naphthalenylboronic acid

Base Information

Chemical Name:5,6,7,8-Tetrahydro-2-naphthalenylboronic acid
CAS No.:405888-56-4
Molecular Formula:C10H13BO2
Molecular Weight:176.02002
Hs Code.:2931900090
Mol file:405888-56-4.mol

Synonyms:5,6,7,8-Tetrahydro-2-naphthalenylboronic acid;5,6,7,8-tetrahydronaphthalen-2-ylboronic acid

Suppliers and Price of 5,6,7,8-Tetrahydro-2-naphthalenylboronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5,6,7,8-Tetrahydro-2-naphthalenylboronicacid
10mg
$ 45.00

Crysdot
(5,6,7,8-Tetrahydronaphthalen-2-yl)boronicacid 95+%
1g
$ 364.00

American Custom Chemicals Corporation
5,6,7,8-TETRAHYDRO-2-NAPHTHALENYLBORONIC ACID 95.00%
5MG
$ 503.80

Alichem
(5,6,7,8-Tetrahydronaphthalen-2-yl)boronicacid
5g
$ 927.00

AK Scientific
5,6,7,8-Tetrahydro-2-naphthalenylboronicacid
10g
$ 1917.00

AK Scientific
5,6,7,8-Tetrahydro-2-naphthalenylboronicacid
250mg
$ 211.00

Total 10 raw suppliers

Chemical Property of 5,6,7,8-Tetrahydro-2-naphthalenylboronic acid

Chemical Property:

Boiling Point:352.1±52.0 °C(Predicted)
PKA:8.91±0.20(Predicted)
PSA：40.46000
Density:1.14±0.1 g/cm3(Predicted)
LogP:0.24520
Storage Temp.:Room temperature.

Purity/Quality:

98% ^*data from raw suppliers

5,6,7,8-Tetrahydro-2-naphthalenylboronicacid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5,6,7,8-Tetrahydro-2-naphthalenylboronic acid

There total 7 articles about 5,6,7,8-Tetrahydro-2-naphthalenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 6134-56-1
6-bromo-1,2,3,4-tetrahydronaphthalene

: 405888-56-4
(5,6,7,8-tetrahydronaphthalen-2-yl)boronic acid

Guidance literature:: 6-bromo-1,2,3,4-tetrahydronaphthalene; With n-butyllithium; In tetrahydrofuran; hexane; for 1.5h; Cooling with acetone-dry ice; Inert atmosphere;

With Triisopropyl borate; In tetrahydrofuran; hexane; for 3.83333h;

With water; ammonium chloride; In tetrahydrofuran; hexane; pH=8; Cooling;

Reference yield: 69.0%

: 119-64-2
tetralin

: 7732-18-5
water

: 13517-10-7
boron triiodide

: 405888-56-4
(5,6,7,8-tetrahydronaphthalen-2-yl)boronic acid

Guidance literature:: tetralin; boron triiodide; at 160 ℃; for 16h; Schlenk technique; Inert atmosphere;

water; With triethylamine; In aq. phosphate buffer; at 20 ℃; for 0.5h; pH=5.8; regioselective reaction;
DOI:10.1021/acs.orglett.9b04483