3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF)

Base Information

Chemical Name:3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF)
CAS No.:1196147-72-4
Molecular Formula:C11H26NP
Molecular Weight:203.304601
Hs Code.:
Mol file:1196147-72-4.mol

Synonyms:3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF);3-(Di-t-butylphosphino)propylaMine;3-(Di-tert-butylphosphino)propylaMine, 10% w/w soln. in THF;3-(Di-t-butylphosphino)propylamine,(10 wt% in THF)

Suppliers and Price of 3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF)
5g
$ 98.00

Strem Chemicals
3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF)
25g
$ 390.00

Alfa Aesar
3-(Di-tert-butylphosphino)propylamine, 10% w/w soln. in THF
25g
$ 266.00

Alfa Aesar
3-(Di-tert-butylphosphino)propylamine, 10% w/w soln. in THF
5g
$ 69.40

Alfa Aesar
3-(Di-tert-butylphosphino)propylamine, 10% w/w soln. in THF
1g
$ 19.50

Total 7 raw suppliers

Chemical Property of 3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF)

Chemical Property:

Boiling Point:259.2±23.0 °C(Predicted)
PKA:10.40±0.10(Predicted)
PSA：39.61000
LogP:4.11440
Sensitive.:Air Sensitive

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF)

There total 2 articles about 3-(Di-t-butylphosphino)propylamine, min. 97% (10 wt% in THF) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 819-19-2
di-tert-butylphosphine

: 180059-71-6
3-chloro-N, N-bis(trimethylsilyl)propylamine

: 1196147-72-4
3-(di-tert-butylphosphine)propylamine

Guidance literature:: di-tert-butylphosphine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2.5h; Inert atmosphere; Schlenk technique;

3-chloro-N, N-bis(trimethylsilyl)propylamine; In tetrahydrofuran; hexane; at -78 - 85 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.8b01815

Reference yield:

: 142132-68-1
Di-tert-butyl-[3-(1,1,1,3,3,3-hexamethyl-disilazan-2-yl)-propyl]-phosphane

: 1196147-72-4
3-(di-tert-butylphosphine)propylamine

Guidance literature:: Di-tert-butyl-[3-(1,1,1,3,3,3-hexamethyl-disilazan-2-yl)-propyl]-phosphane; With sulfuric acid; water; In tetrahydrofuran; at 20 ℃; for 1h;

With sodium hydroxide; In tetrahydrofuran; water; for 1h;
DOI:10.1039/b911459a

Reference yield: 33.0%

: 50982-12-2
cyclooctadiene ruthenium(II) dichloride

: 1196147-72-4
3-(di-tert-butylphosphine)propylamine

: 1196147-60-0
trans-RuCl2((t-Bu)2P(CH2)3NH2)2

Guidance literature:: In dichloromethane; a mixt. of complex and aminophosphine was stirred in CH2Cl2 under Ar for2 h at room temp., then refluxed for 3 h, the mixt. was cooled to room temp.; hexane was added, suspn. was stirred for 1 h, filtered, washed with hexane dried under vac.; elem. anal.;
DOI:10.1039/b911459a