2-{(E)-[2-(4-Methylphenyl)-2-oxoethylidene]amino}benzoic acid

Base Information

Chemical Name:2-{(E)-[2-(4-Methylphenyl)-2-oxoethylidene]amino}benzoic acid
CAS No.:87046-90-0
Molecular Formula:C₁₆H₁₃NO₃
Molecular Weight:267.284
Hs Code.:
NSC Number:166036
DSSTox Substance ID:DTXSID30304508

Synonyms:87046-90-0;NSC166036;DTXSID30304508;2-{(E)-[2-(4-Methylphenyl)-2-oxoethylidene]amino}benzoic acid;NSC-166036

Suppliers and Price of 2-{(E)-[2-(4-Methylphenyl)-2-oxoethylidene]amino}benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-{(E)-[2-(4-Methylphenyl)-2-oxoethylidene]amino}benzoic acid

Chemical Property:

Vapor Pressure:2.96E-10mmHg at 25°C
Boiling Point:485.9°C at 760 mmHg
Flash Point:247.7°C
Density:1.16g/cm³
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:267.08954328
Heavy Atom Count:20
Complexity:383

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C=NC2=CC=CC=C2C(=O)O

Technology Process of 2-{(E)-[2-(4-Methylphenyl)-2-oxoethylidene]amino}benzoic acid

There total 1 articles about 2-{(E)-[2-(4-Methylphenyl)-2-oxoethylidene]amino}benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1075-47-4
4-methylphenylglyoxal

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 87046-90-0
4-methylphenacylidene anthranilic acid

Guidance literature:: In ethanol; for 3.5h; Heating;

Reference yield:

: rhodium(III) chloride trihydrate

: 87046-90-0
4-methylphenacylidene anthranilic acid

: Rh⁽³⁺⁾*2C₁₆H₁₂NO₃^(1-)*Cl^(1-)=Rh(C₁₆H₁₂NO₃)2Cl

Guidance literature:: In ethanol; reflux, 3-4.5 h, stoich. mixt.;

Reference yield:

: 87046-90-0
4-methylphenacylidene anthranilic acid

: 10025-65-7
platinum(II) chloride

: 98628-80-9
[Pt(CH₃C₆H₄C(O)CHNC₆H₄CO₂)Cl]

Guidance literature:: In hydrogenchloride; ethanol; dissoln. of platinum chloride in minimum amt. of hot concd. HCl; diluting with ethanol; addn. of Schiff base ligand (stoichiometric amt.); refluxing on water bath, 4.5 - 5.0 h; refrigeration, a few d; crystn.; washing (water, ethanol, ether); drying in vac.; elem. anal.;