5-Bromo-2-phthalimidopentane

Base Information

• Chemical Name: 5-Bromo-2-phthalimidopentane
• CAS No.: 58554-66-8
• Molecular Formula: C13H14BrNO2
• Molecular Weight: 296.164
• Hs Code.: 2925290090
• Mol file: 58554-66-8.mol

Synonyms:5-Bromo-2-phthalimidopentane;2-(5-bromopentan-2-yl)isoindoline-1,3-dione

Chemical Property of 5-Bromo-2-phthalimidopentane

Chemical Property:

• Boiling Point: 137 °C(Press: 0.06 Torr)
• PKA: -2.21±0.20(Predicted)
• PSA: 37.38000
• Density: 1.474±0.06 g/cm3(Predicted)
• LogP: 2.78410

Purity/Quality:

99% ^*data from raw suppliers

5-Bromo-2-phthalimidopentane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Bromo-2-phthalimidopentane

There total 5 articles about 5-Bromo-2-phthalimidopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthalic anhydride (85-44-9) → N-(4-bromo-1-methyl-butyl)-phthalimide (58554-66-8)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / Beim Erhitzen des Reaktionsprodukts unter vermindertem Druck auf 160grad

2: water; hydrobromic acid / 120 °C

With water; hydrogen bromide; acetic acid;

DOI:10.1021/ja01623a039

Reference yield:

N-(4-hydroxy-1-methyl-butyl)-phthalimide (64992-33-2) → N-(4-bromo-1-methyl-butyl)-phthalimide (58554-66-8)

Guidance literature:

With water; hydrogen bromide; at 120 ℃;

DOI:10.1021/ja01623a039

Reference yield:

(±)-4-amino-1-pentanol (927-55-9) → N-(4-bromo-1-methyl-butyl)-phthalimide (58554-66-8)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / Beim Erhitzen des Reaktionsprodukts unter vermindertem Druck auf 160grad

2: water; hydrobromic acid / 120 °C

With water; hydrogen bromide; acetic acid;

DOI:10.1021/ja01623a039

upstream raw materials:

N-(4-hydroxy-1-methyl-butyl)-phthalimide

phthalic anhydride

(±)-4-amino-1-pentanol

4-nitro-valeric acid ethyl ester