3-(2-PHENYL-1H-INDOL-3-YL)-ACRYLIC ACID ETHYL ESTER

Base Information

• Chemical Name: 3-(2-PHENYL-1H-INDOL-3-YL)-ACRYLIC ACID ETHYL ESTER
• CAS No.: 1017968-62-5
• Molecular Formula: C19H17NO2
• Molecular Weight: 291.349
• Hs Code.: 2933990090
• Mol file: 1017968-62-5.mol

Synonyms:3-(2-PHENYL-1H-INDOL-3-YL)-ACRYLIC ACID ETHYL ESTER;ETHYL 3-(2-PHENYL-1H-3-INDOLYL)-ACRYLATE

Chemical Property of 3-(2-PHENYL-1H-INDOL-3-YL)-ACRYLIC ACID ETHYL ESTER

Chemical Property:

• PSA: 42.09000
• LogP: 4.41120

Purity/Quality:

97% ^*data from raw suppliers

3-(2-PHENYL-1H-INDOL-3-YL)-ACRYLIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2-PHENYL-1H-INDOL-3-YL)-ACRYLIC ACID ETHYL ESTER

There total 2 articles about 3-(2-PHENYL-1H-INDOL-3-YL)-ACRYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-phenyl-indole (948-65-2) + propynoic acid ethyl ester (623-47-2) → (E)-ethyl 3-(2-phenyl-1H-indol-3-yl)propenoate (1017968-62-5)

Guidance literature:

With platinum(II) chloride; In tetrahydrofuran; for 50h; Reflux;

DOI:10.1016/j.tet.2008.11.095

Reference yield: 14.0%

2-phenylethynylaniline (13141-38-3) + propynoic acid ethyl ester (623-47-2) → 2-phenyl-indole (948-65-2) + (E)-ethyl 3-(2-phenyl-1H-indol-3-yl)propenoate (1017968-62-5)

Guidance literature:

With platinum(II) chloride; In tetrahydrofuran; for 24h; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2008.11.095

Reference yield: 67.0%

(E)-ethyl 3-(2-phenyl-1H-indol-3-yl)propenoate (1017968-62-5) → (Z)-ethyl 2-bromo-3-(2-phenyl-1H-indol-3-yl)propenoate (1017968-64-7)

Guidance literature:

With bromine; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

DOI:10.1016/j.tet.2008.01.045

upstream raw materials:

2-phenyl-indole

propynoic acid ethyl ester

2-phenylethynylaniline

Downstream raw materials:

(Z)-ethyl 2-bromo-3-(2-phenyl-1H-indol-3-yl)propenoate

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