N4-(4-METHOXY-PHENYL)-PYRIDINE-3,4-DIAMINE

Base Information

Chemical Name:N4-(4-METHOXY-PHENYL)-PYRIDINE-3,4-DIAMINE
CAS No.:88614-03-3
Molecular Formula:C12H13N3O
Molecular Weight:215.255
Hs Code.:2933399090
Mol file:88614-03-3.mol

Synonyms:N4-(4-METHOXY-PHENYL)-PYRIDINE-3,4-DIAMINE;UKRORGSYN-BB BBV-257959;N4-(4-methoxyphenyl)-3,4-Pyridinediamine

Suppliers and Price of N4-(4-METHOXY-PHENYL)-PYRIDINE-3,4-DIAMINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N4-(4-METHOXY-PHENYL)-PYRIDINE-3,4-DIAMINE

Chemical Property:

PSA：63.40000
LogP:2.41910

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N4-(4-METHOXY-PHENYL)-PYRIDINE-3,4-DIAMINE

There total 6 articles about N4-(4-METHOXY-PHENYL)-PYRIDINE-3,4-DIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 14251-87-7
p. methoxy anilino-4 nitro-3 pyridine

: 88614-03-3
(methoxy-4 anilino)-4 amino-3 pyridine

Guidance literature:: With hydrogen; palladium over charcoal; In ethanol; at 20 ℃; for 18h;

Reference yield: 60.0%

: 14251-87-7
p. methoxy anilino-4 nitro-3 pyridine

: 64-19-7,77671-22-8
acetic acid

: 88614-03-3
(methoxy-4 anilino)-4 amino-3 pyridine

: 92912-16-8
(methoxy-4 anilino)-4 acetamido-3 (1H) pyridone-2

Guidance literature:: With hydrogen; platinum on activated charcoal; at 85 ℃; Mechanism; Product distribution; different catalysators, solvents and temperature were investigated;
DOI:10.1016/S0040-4020(01)83497-9

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 88614-03-3
(methoxy-4 anilino)-4 amino-3 pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / toluene / 16 h / 0 - 110 °C / Heating / reflux

2: sodium hydrogencarbonate / tetrahydrofuran; ethanol / 2 h / 20 - 80 °C

3: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 2585.81 Torr

With hydrogen; sodium hydrogencarbonate; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; toluene;