1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate

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Chemical Name:1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate
CAS No.:850850-61-2
Molecular Formula:C₂₄H₂₇N₇O₄
Molecular Weight:477.523
Hs Code.:

Synonyms:1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate

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Chemical Property of 1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate

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Technology Process of 1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate

There total 6 articles about 1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 607369-54-0
4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenol

: 109384-19-2
t-butyl 4-hydroxy piperidine-1-carboxylate

: 850850-61-2
1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate

Guidance literature:: With di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine; In 1,4-dioxane; at 80 ℃; for 12h;

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 850850-61-2
1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: trichlorophosphate / toluene / 16 h / 0 - 110 °C / Heating / reflux

2.1: sodium hydrogencarbonate / tetrahydrofuran; ethanol / 2 h / 20 - 80 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 2585.81 Torr

4.1: 0.42 h / 195 °C

5.1: hydrogenchloride; sodium nitrite / methanol; water / 1.5 h / 20 °C

5.2: 16 h / 110 °C / pH 11

6.1: boron tribromide / dichloromethane / 16 h / 0 - 20 °C

6.2: pH 14

7.1: di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine / 1,4-dioxane / 12 h / 80 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine; hydrogen; boron tribromide; sodium hydrogencarbonate; sodium nitrite; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; toluene;

Reference yield:

: 14251-87-7
p. methoxy anilino-4 nitro-3 pyridine

: 850850-61-2
1,1-dimethylethyl 4-({4-[2-(4-amino-furazan-3-yl)-1H-imidazo[4,5-c]pyridin-1-yl]phenyl}oxy)-1-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 2585.81 Torr

2.1: 0.42 h / 195 °C

3.1: hydrogenchloride; sodium nitrite / methanol; water / 1.5 h / 20 °C

3.2: 16 h / 110 °C / pH 11

4.1: boron tribromide / dichloromethane / 16 h / 0 - 20 °C

4.2: pH 14

5.1: di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine / 1,4-dioxane / 12 h / 80 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine; hydrogen; boron tribromide; sodium nitrite; palladium 10% on activated carbon; In 1,4-dioxane; methanol; ethanol; dichloromethane; water;