5-(4-Methoxyphenyl)-4-phenyl-1,3,4-thiadiazol-4-ium-2-thiolate

Base Information

• Chemical Name: 5-(4-Methoxyphenyl)-4-phenyl-1,3,4-thiadiazol-4-ium-2-thiolate
• CAS No.: 34009-55-7
• Molecular Formula: C₁₅H₁₂N₂OS₂
• Molecular Weight: 300.405
• Mol file: 34009-55-7.mol

Synonyms:5-(4-Methoxyphenyl)-4-phenyl-1,3,4-thiadiazol-4-ium-2-thiolate

Chemical Property of 5-(4-Methoxyphenyl)-4-phenyl-1,3,4-thiadiazol-4-ium-2-thiolate

Chemical Property:

• Melting Point: 236 °C(Solv: chloroform (67-66-3); ethanol (64-17-5))
• PSA: 87.38000
• LogP: 4.33890

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-(4-Methoxyphenyl)-4-phenyl-1,3,4-thiadiazol-4-ium-2-thiolate

There total 2 articles about 5-(4-Methoxyphenyl)-4-phenyl-1,3,4-thiadiazol-4-ium-2-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium (N'-phenylhydrazino)dithioformate (1007-51-8) + 4-methoxy-benzoyl chloride (100-07-2) → 2-(4-methoxy-phenyl)-3-phenyl-5-thioxo-4,5-dihydro-[1,3,4]thiadiazolium betaine (34009-55-7)

Guidance literature:

In water; Ambient temperature;

DOI:10.1002/jps.2600540515

Reference yield:

potassium (N'-phenylhydrazino)dithioformate (1007-51-8) + 4-methoxybenzoic acid (100-09-4) → 2-(4-methoxy-phenyl)-3-phenyl-5-thioxo-4,5-dihydro-[1,3,4]thiadiazolium betaine (34009-55-7)

Guidance literature:

Multistep reaction; (i) SOCl₂, (ii) /BRN= 4166129/, H₂O;

Reference yield:

2-(4-methoxy-phenyl)-3-phenyl-5-thioxo-4,5-dihydro-[1,3,4]thiadiazolium betaine (34009-55-7) → [1-(4-Methoxy-phenyl)-1-thiocyanato-meth-(E)-ylidene]-phenyl-amine

Guidance literature:

With dimethyl acetylenedicarboxylate; In benzene; Heating;

DOI:10.1039/C3972001300a

upstream raw materials:

potassium (N'-phenylhydrazino)dithioformate

4-methoxy-benzoyl chloride

4-methoxybenzoic acid

Downstream raw materials:

4-methoxy-N-phenylthiobenzamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 34009-55-7 5-(4-Methoxyphenyl)-4-phenyl-1,3,4-thiadiazol-4-ium-2-thiolate

Send

Send

Metric Ton KG G Pound L ML

Send

Send