2-phenylhydrazinecarbodithioic acid

Base Information

• Chemical Name: 2-phenylhydrazinecarbodithioic acid
• CAS No.: 1007-51-8
• Molecular Formula: C7H8 N2 S2 . K
• Molecular Weight: 222.376
• Mol file: 1007-51-8.mol

Synonyms:Carbazicacid, 3-phenyldithio-, monopotassium salt (8CI); Carbazic acid,3-phenyldithio-, potassium salt (7CI); Hydrazinecarbodithioic acid, 2-phenyl-,monopotassium salt (9CI); 2-Phenylhydrazinecarbodithioic acid monopotassiumsalt; Potassium 3-phenyldithiocarbazate

Chemical Property of 2-phenylhydrazinecarbodithioic acid

Chemical Property:

• Vapor Pressure: 0.00704mmHg at 25°C
• Boiling Point: 270°Cat760mmHg
• Flash Point: 117.1°C
• Density: 1.347g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-phenylhydrazinecarbodithioic acid

There total 2 articles about 2-phenylhydrazinecarbodithioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + phenylhydrazine (100-63-0) → potassium (N'-phenylhydrazino)dithioformate (1007-51-8)

Guidance literature:

With potassium hydroxide; Yield given. Multistep reaction; 1.) ethanol, 0 deg C, 1 min, 2.) ethanol, 4 deg C, 4 h;

Reference yield:

ethanol (64-17-5) + phenylhydrazine (100-63-0) → potassium (N'-phenylhydrazino)dithioformate (1007-51-8)

Guidance literature:

in der Kaelte;

Reference yield: 93.0%

potassium (N'-phenylhydrazino)dithioformate (1007-51-8) + α-bromoacetophenone (70-11-1) → phenacyl (N'-phenylhydrazino)dithioformate (14580-26-8)

Guidance literature:

In ethanol; water; at 4 ℃; for 16h;

upstream raw materials:

carbon disulfide

phenylhydrazine

ethanol

Downstream raw materials:

3-phenyl-5-thioxo-[1,3,4]thiadiazolidin-2-one

(4'-nitro)benzyl 3-phenyl dithiocarbazate

bis-(3-phenyl-thiohydrazinocarbonyl)-disulfane

diphenyl thiocarbazide