Cyclopropanecarboxylic acid, 2-butyl-, methyl ester, (1S,2S)- (9CI)

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 2-butyl-, methyl ester, (1S,2S)- (9CI)
CAS No.:210546-53-5
Molecular Formula:C₉H₁₆O₂
Molecular Weight:156.225
Hs Code.:
Mol file:210546-53-5.mol

Synonyms:Cyclopropanecarboxylic acid, 2-butyl-, methyl ester, (1S,2S)- (9CI)

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Chemical Property of Cyclopropanecarboxylic acid, 2-butyl-, methyl ester, (1S,2S)- (9CI)

Chemical Property:

PSA：26.30000
LogP:1.98570

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Cyclopropanecarboxylic acid, 2-butyl-, methyl ester, (1S,2S)- (9CI)

There total 9 articles about Cyclopropanecarboxylic acid, 2-butyl-, methyl ester, (1S,2S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 210546-52-4
(1R,2S)-2-Butyl-cyclopropanecarboxylic acid methyl ester

: 210546-53-5
Methyl (1S,2S)-2-butylcyclopropanecarboxylate

Guidance literature:: With potassium hexamethylsilazane;
DOI:10.1016/S0040-4039(98)00759-X

Reference yield:

: 67-56-1
methanol

: 1-(2-Butylcyclopropyl)methanoic acid

: 210546-53-5
Methyl (1S,2S)-2-butylcyclopropanecarboxylate

: Methyl (1R,2R)-2-butylcyclopropanecarboxylate

Guidance literature:: With sulfuric acid; at 20 ℃; for 48h; Title compound not separated from byproducts;
DOI:10.1002/(SICI)1521-3765(19990702)5:7<2055::AID-CHEM2055>3.0.CO;2-9

Reference yield:

: 112947-70-3
1-(trimethylsilyl)-2-heptyn-1-one

: 210546-53-5
Methyl (1S,2S)-2-butylcyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / (-)-B-chloro diisopinocamphenylborane

2: H₂ / Lindlar catalyst

3: 97 percent / Et₂Zn

4: Swern oxidation

5: H₂O₂, NaOH

6: 86 percent

7: 56 percent / KHMDS

With sodium hydroxide; hydrogen; dihydrogen peroxide; diethylzinc; potassium hexamethylsilazane; (-)-diisopinocamphenylborane chloride; Lindlar's catalyst;
DOI:10.1016/S0040-4039(98)00759-X