1,3,5-Triphenoxybenzene

Base Information

• Chemical Name: 1,3,5-Triphenoxybenzene
• CAS No.: 23879-81-4
• Molecular Formula: C24H18O3
• Molecular Weight: 354.4
• Hs Code.: 2909309090
• Mol file: 23879-81-4.mol

Synonyms:1,3,5-Triphenoxybenzene

Chemical Property of 1,3,5-Triphenoxybenzene

Chemical Property:

• Melting Point: 108 - 110 °C
• PSA: 27.69000
• LogP: 7.06350

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-Triphenoxybenzene

There total 8 articles about 1,3,5-Triphenoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1,3,5-trisbromobenzene (626-39-1) + phenol (108-95-2,27073-41-2) → triphenyl phloroglucinol ether (23879-81-4)

Guidance literature:

With copper(l) iodide; caesium carbonate; In 1-methyl-pyrrolidin-2-one; at 160 ℃; for 16h;

DOI:10.1016/j.tetlet.2007.08.026

Reference yield:

1-Nitro-3,5-diphenoxy-benzene + phenol (108-95-2,27073-41-2) → triphenyl phloroglucinol ether (23879-81-4)

Guidance literature:

With potassium carbonate; In various solvent(s); at 200 ℃; for 2h;

DOI:10.1007/BF00702161

Reference yield:

1,3,5-trichlorobenzene (108-70-3,63697-19-8) + phenol (108-95-2,27073-41-2) → triphenyl phloroglucinol ether (23879-81-4)

Guidance literature:

phenol; With sodium hydride; In 1,4-dioxane; at 20 ℃; for 1h;

1,3,5-trichlorobenzene; In 1,4-dioxane; at 100 ℃; for 10h;

DOI:10.1039/c7cc06717h

upstream raw materials:

1,3,5-trisbromobenzene

phenol

potassium phenolate

1,3,5-trinitrobenzene