(4-Ethoxy-2,6-difluorophenyl)methanol

Base Information

• Chemical Name: (4-Ethoxy-2,6-difluorophenyl)methanol
• CAS No.: 438050-23-8
• Molecular Formula: C9H10F2O2
• Molecular Weight: 188.17
• Hs Code.: 2909498090
• Mol file: 438050-23-8.mol

Synonyms:(4-Ethoxy-2,6-difluorophenyl)methanol;4-Ethoxy-2,6-difluorobenzylalcohol

Chemical Property of (4-Ethoxy-2,6-difluorophenyl)methanol

Chemical Property:

• Boiling Point: 230.8±35.0 °C(Predicted)
• PKA: 13.48±0.10(Predicted)
• PSA: 29.46000
• Density: 1.236±0.06 g/cm3(Predicted)
• LogP: 1.85580

Purity/Quality:

99% ^*data from raw suppliers

4-Ethoxy-2,6-difluorobenzyl alcohol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4-Ethoxy-2,6-difluorophenyl)methanol

There total 2 articles about (4-Ethoxy-2,6-difluorophenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

ethyl bromide (74-96-4) + 3,5-difluoro-4-(hydroxymethyl)phenol → 4-ethoxy-2,6-difluoro-benzylalcohol (438050-23-8)

Guidance literature:

Reference yield:

4-ethoxy-2,6-difluorobenzaldehyde (1017779-48-4) → 4-ethoxy-2,6-difluoro-benzylalcohol (438050-23-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃;

DOI:10.1016/j.bmcl.2012.11.115

Reference yield: 81.0%

4-ethoxy-2,6-difluoro-benzylalcohol (438050-23-8) + (R)-4-chlorocarbonyl-3-ethyl-piperazine-1-carboxylic acid tert-butyl ester (438050-09-0) → (R)-2-ethyl-piperazine-1,4-dicarboxylic acid 4-tert-butyl ester 1-(4-ethoxy-2,6-difluoro-benzyl)ester (438050-24-9)

Guidance literature:

upstream raw materials:

ethyl bromide

4-ethoxy-2,6-difluorobenzaldehyde

Downstream raw materials:

(R)-2-ethyl-piperazine-1,4-dicarboxylic acid 4-tert-butyl ester 1-(4-ethoxy-2,6-difluoro-benzyl)ester

2-(bromomethyl)-5-ethoxy-1,3-difluorobenzene

C₁₀H₉F₂NO

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