Ethyl -Ethoxycarbonyl--oxo-3-pyridinebutyrate

Base Information

• Chemical Name: Ethyl -Ethoxycarbonyl--oxo-3-pyridinebutyrate
• CAS No.: 54109-95-4
• Molecular Formula: C14H17NO5
• Molecular Weight: 278.28054
• Hs Code.: 2933399090
• Mol file: 54109-95-4.mol

Synonyms:Ethyl -Ethoxycarbonyl--oxo-3-pyridinebutyrate;2-(3-Pyridinylcarbonyl)butanedioic Acid 1,4-Diethyl Ester;Diethyl 2-(Pyridin-3-ylcarbonyl)succinate

Chemical Property of Ethyl -Ethoxycarbonyl--oxo-3-pyridinebutyrate

Chemical Property:

• Boiling Point: 154-156°C @0.7mmHg
• PSA: 82.56000
• LogP: 1.39680
• Solubility.: Chloroform, Ether

Purity/Quality:

97% ^*data from raw suppliers

Ethylβ-Ethoxycarbonyl-γ-oxo-3-pyridinebutyrate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Ethyl β-Ethoxycarbonyl-γ-oxo-3-pyridinebutyrate (cas# 54109-95-4) is a compound useful in organic synthesis.

Technology Process of Ethyl -Ethoxycarbonyl--oxo-3-pyridinebutyrate

There total 3 articles about Ethyl -Ethoxycarbonyl--oxo-3-pyridinebutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

3-pyridinecarboxylic acid ethyl ester (614-18-6) + succinic acid diethyl ester (123-25-1) → diethyl 3-pyridylcarbonylsuccinate (54109-95-4)

Guidance literature:

With sodium hydride; In diethyl ether; at 20 ℃; for 48h;

Reference yield:

3-oxo-3-pyridin-3-yl-propionic acid ethyl ester (6283-81-4) + ethyl bromoacetate (105-36-2) → diethyl 3-pyridylcarbonylsuccinate (54109-95-4)

Guidance literature:

With ethanol; potassium ethoxide;

DOI:10.1248/cpb1953.2.39

Reference yield:

→ diethyl 3-pyridylcarbonylsuccinate (54109-95-4)

Guidance literature:

Pyridin-3-carbonsaeure-ethylester, Diethylsuccinat, NaH;

DOI:10.1002/ardp.19743070907

upstream raw materials:

3-pyridinecarboxylic acid ethyl ester

succinic acid diethyl ester

3-oxo-3-pyridin-3-yl-propionic acid ethyl ester

ethyl bromoacetate

Downstream raw materials:

4-oxo-4-(pyridin-3-yl)butanoic acid

ethyl 4-oxo-4-(pyridin-3-yl)butanoate

C₁₂H₁₃NO₅

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