3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo(a,d)cycloheptene

Base Information

Chemical Name:3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo(a,d)cycloheptene
CAS No.:146364-05-8
Molecular Formula:C₁₆H₁₄FN
Molecular Weight:239.292
Hs Code.:
Mol file:146364-05-8.mol

Synonyms:10,5-(Iminomethano)-5H-dibenzo[a,d]cycloheptene,3-fluoro-10,11-dihydro-, (?à)-

Suppliers and Price of 3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo(a,d)cycloheptene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-FLUORO-10,5-(IMINOMETHANO)-10,11-DIHYDRO-5H-DIBENZO(A,D)CYCLOHEPTENE 95.00%
5MG
$ 505.34

Total 1 raw suppliers

Chemical Property of 3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo(a,d)cycloheptene

Chemical Property:

Boiling Point:343.8±42.0 °C(Predicted)
PKA:8?+-.0.20(Predicted)
Density:1.193±0.06 g/cm3(Predicted)

Purity/Quality:: 3-FLUORO-10,5-(IMINOMETHANO)-10,11-DIHYDRO-5H-DIBENZO(A,D)CYCLOHEPTENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo(a,d)cycloheptene

There total 6 articles about 3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo(a,d)cycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 347-91-1
2-(4-fluorophenyl)-1-phenylethanone

: 146364-05-8
3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo[a,d]cycloheptene

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / Ambient temperature

2: borane-tetrahydrofuran complex / 3 h / Heating

3: potassium carbonate / dimethylformamide / 16 h / 100 °C

4: perchloric acid / 24 h / Ambient temperature

With pyridine; perchloric acid; borane-THF; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00066a002

Reference yield:

: 133235-88-8,133235-90-2,74533-87-2
2-(4-fluoro-phenyl)-1-phenyl-ethylamine

: 146364-05-8
3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo[a,d]cycloheptene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethylformamide / 16 h / 100 °C

2: perchloric acid / 24 h / Ambient temperature

With perchloric acid; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00066a002

Reference yield:

: 2-(4-Fluoro-phenyl)-1-phenyl-ethanone O-methyl-oxime

: 146364-05-8
3-fluoro-10,5-(iminomethano)-10,11-dihydro-5H-dibenzo[a,d]cycloheptene

Guidance literature:: Multi-step reaction with 3 steps

1: borane-tetrahydrofuran complex / 3 h / Heating

2: potassium carbonate / dimethylformamide / 16 h / 100 °C

3: perchloric acid / 24 h / Ambient temperature

With perchloric acid; borane-THF; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00066a002