Technology Process of 4-[1-(2-methoxyethyl)-4-piperidinyl]Benzoic acid hydrochloride
There total 4 articles about 4-[1-(2-methoxyethyl)-4-piperidinyl]Benzoic acid hydrochloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
at 90 ℃;
for 24h;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,4-dioxane; water / 24 h / 100 °C
2: 20% palladium hydroxide-activated charcoal; hydrogen / methanol / 1500.15 Torr
3: potassium carbonate / acetonitrile / 24 h / 90 °C / Sealed tube
With
bis-triphenylphosphine-palladium(II) chloride; 20% palladium hydroxide-activated charcoal; hydrogen; sodium carbonate; potassium carbonate;
In
1,4-dioxane; methanol; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,4-dioxane; water / 24 h / 100 °C
2: 20% palladium hydroxide-activated charcoal; hydrogen / methanol / 1500.15 Torr
3: potassium carbonate / acetonitrile / 24 h / 90 °C / Sealed tube
With
bis-triphenylphosphine-palladium(II) chloride; 20% palladium hydroxide-activated charcoal; hydrogen; sodium carbonate; potassium carbonate;
In
1,4-dioxane; methanol; water; acetonitrile;
