22α-Ethyl-15,16-dimethoxy-25-acetyl-4,25-secoobscurinervan-4β-ol

Base Information

Chemical Name:22α-Ethyl-15,16-dimethoxy-25-acetyl-4,25-secoobscurinervan-4β-ol
CAS No.:72101-38-3
Molecular Formula:C₂₇H₃₈N₂O₆
Molecular Weight:486.609
Hs Code.:
Mol file:72101-38-3.mol

Synonyms:22α-Ethyl-15,16-dimethoxy-25-acetyl-4,25-secoobscurinervan-4β-ol

Suppliers and Price of 22α-Ethyl-15,16-dimethoxy-25-acetyl-4,25-secoobscurinervan-4β-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 22α-Ethyl-15,16-dimethoxy-25-acetyl-4,25-secoobscurinervan-4β-ol

Chemical Property:

Melting Point:179 - 180 °C (hexane)
PSA：80.70000
LogP:2.87640

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 22α-Ethyl-15,16-dimethoxy-25-acetyl-4,25-secoobscurinervan-4β-ol

There total 3 articles about 22α-Ethyl-15,16-dimethoxy-25-acetyl-4,25-secoobscurinervan-4β-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7097-00-9
obscurinervine

: 72101-38-3
21-acetoxy-5'α-ethyl-15,16-dimethoxy-5',6'-dihydro-[1,4]oxazino[4',3',2':1,18,17]aspidospermidin-4β-ol

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd-C / ethyl acetate

2: LiAlH₄ / diethyl ether / Heating

3: benzene / 1 h / 0 °C

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; ethyl acetate; benzene;
DOI:10.1021/ja01066a031

Reference yield:

: 7097-01-0
obscurinervine

: 72101-38-3
21-acetoxy-5'α-ethyl-15,16-dimethoxy-5',6'-dihydro-[1,4]oxazino[4',3',2':1,18,17]aspidospermidin-4β-ol

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / Heating

2: benzene / 1 h / 0 °C

With lithium aluminium tetrahydride; In diethyl ether; benzene;
DOI:10.1021/ja01066a031