Acetaldehyde diethyl hydrazone

Base Information

• Chemical Name: Acetaldehyde diethyl hydrazone
• CAS No.: 7422-91-5
• Molecular Formula: C6H14N2
• Molecular Weight: 0
• Mol file: 7422-91-5.mol

Synonyms:Acetaldehyde diethyl hydrazone

Chemical Property of Acetaldehyde diethyl hydrazone

Chemical Property:

• PSA: 15.60000
• LogP: 1.33390

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetaldehyde diethyl hydrazone

There total 7 articles about Acetaldehyde diethyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.2%

1-ethyl-2-(propan-2-ylidene)hydrazine (7422-99-3) + 1,1-diethyldiazenium bromide → aldehyde diethylhydrazone (7422-91-5) + tetraethyl-2-tetrazene (13304-29-5) + Aceton-diaethylhydrazon (16713-36-3) + 3,3-dimethyl-1,5,5-triethyl-3,4-dihydroformazan

Guidance literature:

With triethylamine; at -30 - -20 ℃; Further byproducts given. Title compound not separated from byproducts;

Reference yield:

N,N-diethylhydrazine (616-40-0) + acetaldehyde (75-07-0,9002-91-9) → aldehyde diethylhydrazone (7422-91-5)

Guidance literature:

With water;

Reference yield:

N-Nitrosodiethylamine (55-18-5) → aldehyde diethylhydrazone (7422-91-5)

Guidance literature:

With acetic acid; zinc;

upstream raw materials:

ethylmagnesium iodide

diethyl ether

N-Nitrosodiethylamine

N,N-diethylhydrazine

Downstream raw materials:

1,1-Diethyl-2-isopropylhydrazin

1,1-Diethyl-2-sek-hexylhydrazin

Refernces

• 1、 Kuznetsov, M. A.,Kuznetsova, L. M.,Zasukhina, E. A.. "REACTIONS OF 1,1-DIALKYLDIAZENIUM SALTS WITH KETONE ETHYLHYDRAZONES". . p. 1363 - 1366. Retrieved 2007/10/02.