EthanaMine, 2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)-

Base Information

Chemical Name:EthanaMine, 2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)-
CAS No.:1029134-74-4
Molecular Formula:C₁₃H₁₅NO
Molecular Weight:201.268
Hs Code.:
Mol file:1029134-74-4.mol

Synonyms:EthanaMine, 2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)-

Suppliers and Price of EthanaMine, 2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of EthanaMine, 2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)-

Chemical Property:

PSA：35.25000
LogP:2.61010

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of EthanaMine, 2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)-

There total 2 articles about EthanaMine, 2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 221530-44-5
2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)acetonitrile

: 1029134-74-4
C₁₃H₁₅NO

Guidance literature:: With ammonia; hydrogen; In ethanol; at 20 ℃; for 72h;
DOI:10.1021/jm200221q

Reference yield:

: 196597-78-1
1,2,6,7-tetrahydro-8H-indeno[5,4-b]-furan-8-one

: 1029134-74-4
C₁₃H₁₅NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

1.2: 1 h / 40 °C

2.1: ammonia; hydrogen / ethanol / 72 h / 20 °C

With ammonia; hydrogen; sodium hydride; In tetrahydrofuran; ethanol; mineral oil; 1.1: Horner-Wadsworth-Emmons olefination / 1.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jm200221q

Reference yield:

: 1029134-74-4
C₁₃H₁₅NO

: 1287785-26-5
N-(2-[7-(3-isopropylphenyl)-1,6-dihydro-2H-indeno[5,4-b]-furan-8-yl]ethyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / methanol; ethyl acetate / 3 h / 60 °C

2: triethylamine / dichloromethane / 0.17 h / 20 °C

3: bromine / dichloromethane / 0.5 h / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 0.5 h / 80 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; sodium carbonate; triethylamine; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; 4: Suzuki coupling;
DOI:10.1021/jm200221q