1-Cyclohexyl-1H-benzo[d][1,2,3]triazole

Base Information

Chemical Name:1-Cyclohexyl-1H-benzo[d][1,2,3]triazole
CAS No.:66536-70-7
Molecular Formula:C₁₂H₁₅N₃
Molecular Weight:201.271
Hs Code.:
DSSTox Substance ID:DTXSID60871455
Nikkaji Number:J684.266F

Synonyms:1-Cyclohexyl-1H-benzo[d][1,2,3]triazole;66536-70-7;1-Cyclohexyl-1H-benzotriazole;DTXSID60871455;1-cyclohexyl-1H-1,2,3-benzotriazole

Suppliers and Price of 1-Cyclohexyl-1H-benzo[d][1,2,3]triazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-Cyclohexyl-1H-benzo[d][1,2,3]triazole

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:201.126597491
Heavy Atom Count:15
Complexity:213

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)N2C3=CC=CC=C3N=N2

Technology Process of 1-Cyclohexyl-1H-benzo[d][1,2,3]triazole

There total 9 articles about 1-Cyclohexyl-1H-benzo[d][1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1365271-85-7
1-cyclohexyl-6-fluoro-1H-benzo[d][1,2,3]triazole

: 66536-70-7
1-cyclohexyl-1Hbenzo[d][1,2,3]triazole

Guidance literature:: With 2-methyl-propan-1-ol; methanesulfonato(2-dicyclohexylphosphino -2’,6’-di-i-propoxy-1,1‘-biphenyl)(2’-amino-1,1’-biphenyl-2-yl)palladium(II); sodium tert-pentoxide; In toluene; at 80 ℃; for 18h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.9b00889

Reference yield: 80.0%

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 98-89-5
Cyclohexanecarboxylic acid

: 66536-70-7
1-cyclohexyl-1Hbenzo[d][1,2,3]triazole

Guidance literature:: With copper(I) thiophene-2-carboxylate; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(5-methyl-2-(4-fluorophenyl)pyridine(-1H))-iridium(III) hexafluorophosphate; N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; bathophenanthroline; iodomesitylene diacetate; In 1,4-dioxane; at 20 ℃; for 1h; Reagent/catalyst; regioselective reaction; Inert atmosphere; Irradiation;
DOI:10.1038/s41586-018-0234-8

Reference yield: 35.0%

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 110-82-7,25012-93-5
cyclohexane

: 66536-70-7
1-cyclohexyl-1Hbenzo[d][1,2,3]triazole

Guidance literature:: With 1,10-Phenanthroline; copper(I) bromide dimethylsulfide complex; di-tert-butyl peroxide; In tert-butyl alcohol; at 135 ℃; for 15h; Schlenk technique;
DOI:10.1002/cssc.201700783