D-glycero-L-manno-2-Nonulose, 4,8-anhydro-1,3-dideoxy- (9CI)

Base Information

• Chemical Name: D-glycero-L-manno-2-Nonulose, 4,8-anhydro-1,3-dideoxy- (9CI)
• CAS No.: 469873-52-7
• Molecular Formula: C9H16O6
• Molecular Weight: 220.222
• Mol file: 469873-52-7.mol

Synonyms:D-glycero-L-manno-2-Nonulose, 4,8-anhydro-1,3-dideoxy- (9CI)

Chemical Property of D-glycero-L-manno-2-Nonulose, 4,8-anhydro-1,3-dideoxy- (9CI)

Chemical Property:

• Melting Point: 169 - 171 °C
• PSA: 107.22000
• LogP: -2.19210

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of D-glycero-L-manno-2-Nonulose, 4,8-anhydro-1,3-dideoxy- (9CI)

There total 8 articles about D-glycero-L-manno-2-Nonulose, 4,8-anhydro-1,3-dideoxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

5,6,7,9-tetra-O-acetyl-4,8-anhydro-1,3-dideoxy-D-glycero-L-gluco-nonulose (853269-40-6) → 4,8-anhydro-1,3-dideoxy-D-glycero-L-gluco-nonulose (469873-52-7)

Guidance literature:

With methanol; sodium methylate; at 20 ℃;

DOI:10.1016/j.bmc.2008.06.044

Reference yield: 92.0%

D-Galactose (10257-28-0) + acetylacetone (123-54-6,81235-32-7) → 4,8-anhydro-1,3-dideoxy-D-glycero-L-gluco-nonulose (469873-52-7)

Guidance literature:

With sodium hydrogencarbonate; In water; at 90 ℃; for 8h;

DOI:10.1080/07328300701609111

Reference yield: 85.0%

D-Galactose (10257-28-0) + dimethyl (2-oxopropyl)phosphonate (4202-14-6) → 4,8-anhydro-1,3-dideoxy-D-glycero-L-gluco-nonulose (469873-52-7)

Guidance literature:

With potassium carbonate; In water; at 60 ℃; for 24h;

DOI:10.1007/s11426-010-4055-3

upstream raw materials:

D-Galactose

acetylacetone

5,6,7,9-tetra-O-acetyl-4,8-anhydro-1,3-dideoxy-D-glycero-L-gluco-nonulose

dimethyl (2-oxopropyl)phosphonate

Downstream raw materials:

4-butyl-5-pentyl-2-((2S,3R,4R,5R,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)cyclohex-2-enone

(E)-1-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-4-(3-hydroxyphenyl)but-3-en-2-one

(E)-1-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-4-(4-hydroxyphenyl)but-3-en-2-one

(E)-1-β-D-galactopyranosyl-4-(3-hydroxyphenyl)but-3-en-2-one

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