N-Boc-5-Methoxy-7-Methylindole, 97%

Base Information

Chemical Name:N-Boc-5-Methoxy-7-Methylindole, 97%
CAS No.:1387445-50-2
Molecular Formula:C₁₅H₁₉NO₃
Molecular Weight:261.321
Hs Code.:
Mol file:1387445-50-2.mol

Synonyms:N-Boc-5-Methoxy-7-Methylindole, 97%;tert-butyl 5-methoxy-7-methyl-1H-indole-1-carboxylate

Suppliers and Price of N-Boc-5-Methoxy-7-Methylindole, 97%

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Ambeed
tert-Butyl5-methoxy-7-methyl-1H-indole-1-carboxylate 97%
250mg
$ 32.00

Ambeed
tert-Butyl5-methoxy-7-methyl-1H-indole-1-carboxylate 97%
5g
$ 275.00

Ambeed
tert-Butyl5-methoxy-7-methyl-1H-indole-1-carboxylate 97%
1g
$ 92.00

Alfa Aesar
N-Boc-5-methoxy-7-methylindole, 97%
5g
$ 328.00

Alfa Aesar
N-Boc-5-methoxy-7-methylindole, 97%
1g
$ 82.10

Alfa Aesar
N-Boc-5-methoxy-7-methylindole, 97%
250mg
$ 27.30

Total 9 raw suppliers

Chemical Property of N-Boc-5-Methoxy-7-Methylindole, 97%

Chemical Property:

PSA：40.46000
LogP:3.74150
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl5-methoxy-7-methyl-1H-indole-1-carboxylate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-Boc-5-Methoxy-7-Methylindole, 97%

There total 1 articles about N-Boc-5-Methoxy-7-Methylindole, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 61019-05-4
5-methoxy-7-methyl-1H-indole

: 24424-99-5
di-tert-butyl dicarbonate

: 1387445-50-2
tert-butyl 5-methoxy-7-methyl-1H-indole-1-carboxylate

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 50 ℃; for 5h;
DOI:10.1021/acs.jmedchem.9b01870

Reference yield:

: 1387445-50-2
tert-butyl 5-methoxy-7-methyl-1H-indole-1-carboxylate

: (-)-4-((2S,4S)-4-methoxy-1-((5-methoxy-7-methyl-1H-indol-4-yl)methyl)piperidin-2-yl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride / dichloromethane / 16.5 h / 20 °C / Inert atmosphere

1.2: 2.25 h / -14 °C

2.1: sodium tris(acetoxy)borohydride / trans-1,2-dichloroethylene / 72 h / 20 °C / Inert atmosphere

2.2: 22 h / 70 °C

With oxalyl dichloride; sodium tris(acetoxy)borohydride; In trans-1,2-dichloroethylene; dichloromethane;

Reference yield:

: 1387445-50-2
tert-butyl 5-methoxy-7-methyl-1H-indole-1-carboxylate

: (±)-tert-butyl 5-methoxy-4-(rel-(2S,4S)-(4-methoxy-2-(4-(methoxycarbonyl)phenyl)piperidin-1-yl)methyl)-7-methyl-1H-indole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride / dichloromethane / 16.5 h / 20 °C / Inert atmosphere

1.2: 2.25 h / -14 °C

2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 17 h / 20 °C / Inert atmosphere

With oxalyl dichloride; sodium tris(acetoxy)borohydride; In dichloromethane; 1,2-dichloro-ethane;