(2-bromophenyl)carbonylmorpholine

Base Information

• Chemical Name: (2-bromophenyl)carbonylmorpholine
• CAS No.: 209962-07-2
• Molecular Formula: C₁₁H₁₂BrNO₂
• Molecular Weight: 270.126
• Hs Code.: 2934999090
• Mol file: 209962-07-2.mol

Synonyms:(2-Bromophenyl)(morpholino)methanone;(2-bromophenyl)carbonylmorpholine;2-Bromo-1-(morpholinocarbonyl)benzene

Chemical Property of (2-bromophenyl)carbonylmorpholine

Chemical Property:

• PSA: 29.54000
• LogP: 1.85940
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-1-(morpholinocarbonyl)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-bromophenyl)carbonylmorpholine

There total 6 articles about (2-bromophenyl)carbonylmorpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

morpholine (110-91-8,99108-56-2) + 2-bromobenzoic acid ethyl ester (6091-64-1) → (2-bromophenyl)(morpholino)methanone (209962-07-2)

Guidance literature:

morpholine; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at 0 ℃; for 3h; Inert atmosphere;

2-bromobenzoic acid ethyl ester; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1016/j.tet.2014.03.045

Reference yield: 65.0%

morpholine (110-91-8,99108-56-2) + carbon monoxide (201230-82-2) + 2-(trifluoromethanesulfonyl)oxy-bromobenzene (129112-25-0) → (2-bromophenyl)(morpholino)methanone (209962-07-2)

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; N-ethyl-N,N-diisopropylamine; In toluene; at 90 ℃; for 24h; under 3750.38 Torr; chemoselective reaction; Autoclave; Inert atmosphere;

DOI:10.1002/chem.201702015

Reference yield: 64.0%

morpholine (110-91-8,99108-56-2) + ortho-bromobenzaldehyde (6630-33-7) → (2-bromophenyl)(morpholino)methanone (209962-07-2)

Guidance literature:

With styrene; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; cesium acetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In water; benzene; at 80 ℃; for 24h;

DOI:10.1039/c5sc03103f

upstream raw materials:

morpholine

2-bromobenzoic acid ethyl ester

ortho-bromobenzaldehyde

2-bromobenzoic acid chloride

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