Bis(2-methylallyl)malonic acid dimethyl ester

Base Information

Chemical Name:Bis(2-methylallyl)malonic acid dimethyl ester
CAS No.:74793-47-8
Molecular Formula:C13H20O4
Molecular Weight:0
Hs Code.:
Mol file:74793-47-8.mol

Synonyms:2,2-Bis(2-methyl-2-propenyl)malonic acid dimethyl ester;Bis(2-methyl-2-propenyl)malonic acid dimethyl ester;Bis(2-methyl-2-propenyl)propanedioic acid dimethyl ester;Bis(2-methylallyl)malonic acid dimethyl ester

Suppliers and Price of Bis(2-methylallyl)malonic acid dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Bis(2-methylallyl)malonic acid dimethyl ester

Chemical Property:

PSA：52.60000
LogP:2.25120

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Bis(2-methylallyl)malonic acid dimethyl ester

There total 4 articles about Bis(2-methylallyl)malonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 820-71-3
methallyl acetate

: 108-59-8
malonic acid dimethyl ester

: 74793-47-8
dimethyl 2,2-di(2-methylallyl)malonate

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; N,O-bis-(trimethylsilyl)-acetamide; 1,3-bis-(diphenylphosphino)propane; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/0040-4039(96)01302-0

Reference yield: 86.0%

: 1458-98-6
2-methyl-3-bromo-1-propene

: 108-59-8
malonic acid dimethyl ester

: 74793-47-8
dimethyl 2,2-di(2-methylallyl)malonate

Guidance literature:: malonic acid dimethyl ester; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -20 ℃; for 0.5h; Inert atmosphere;

2-methyl-3-bromo-1-propene; In N,N-dimethyl-formamide; mineral oil; at -20 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/adsc.201500573

Reference yield: 74.0%

: 108-59-8
malonic acid dimethyl ester

: 563-47-3
3-Chloro-2-methylpropene

: 50598-40-8
dimethyl (2-methyl-2-propenyl)-propanedioate

: 74793-47-8
dimethyl 2,2-di(2-methylallyl)malonate

Guidance literature:: malonic acid dimethyl ester; With sodium methylate; potassium iodide; In methanol; at 20 ℃; for 1h; Inert atmosphere;

3-Chloro-2-methylpropene; In methanol; at 20 ℃; Reflux; Inert atmosphere;