Difluorophosphine sulfide

Base Information

• Chemical Name: Difluorophosphine sulfide
• CAS No.: 13780-63-7
• Molecular Formula: F2HPS
• Molecular Weight: 102.045
• Mol file: 13780-63-7.mol

Synonyms:Difluorophosphine sulfide;

Chemical Property of Difluorophosphine sulfide

Chemical Property:

• PSA: 55.56000
• LogP: 2.08210

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Difluorophosphine sulfide

There total 6 articles about Difluorophosphine sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

chlorogermane (13637-65-5) + bis(difluorophosphino) sulphide (24331-65-5) → germane (7782-65-2) + difluoro(germylthio)phosphine (39491-87-7) + chlorodifluorophosphine (14335-40-1) + difluorophosphine sulfide (13780-63-7)

Guidance literature:

mixt. was warmed to 209 K for 2 h; examined by NMR, sepd. by fractional condensation;

DOI:10.1007/BF00938730

Reference yield:

difluoro(germylthio)phosphine (39491-87-7) → chlorogermane (13637-65-5) + difluorophosphine sulfide (13780-63-7)

Guidance literature:

With HCl; mixt. was warmed to room temp. for 5 min; sepd. by fractional condensation; IR, NMR;

DOI:10.1007/BF00938730

Reference yield:

difluoro(germylthio)phosphine (39491-87-7) → bromogermanate (13569-43-2) + difluorophosphine sulfide (13780-63-7)

Guidance literature:

With HBr; mixt. was warmed to room temp. for 5 min; sepd. by fractional condensation; IR, NMR;

DOI:10.1007/BF00938730

upstream raw materials:

bromodifluorophosphine

hydrogen sulfide

bis(difluorophosphino) sulphide

bis(difluorophosphino) seleniede

Downstream raw materials:

carbonyldihydridotris(triphenylphosphine)iridium(I) difluorophosphine sulphide

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