2-(4-Cyclopropoxy-phenyl)-4,4,5,5-tetraMethyl-[1,3,2]dioxaborolane

Base Information

Chemical Name:2-(4-Cyclopropoxy-phenyl)-4,4,5,5-tetraMethyl-[1,3,2]dioxaborolane
CAS No.:1398503-71-3
Molecular Formula:C15H21BO3
Molecular Weight:260.141
Hs Code.:2931900090
Mol file:1398503-71-3.mol

Synonyms:2-(4-Cyclopropoxy-phenyl)-4,4,5,5-tetraMethyl-[1,3,2]dioxaborolane

Suppliers and Price of 2-(4-Cyclopropoxy-phenyl)-4,4,5,5-tetraMethyl-[1,3,2]dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(4-Cyclopropoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
100mg
$ 100.00

Crysdot
2-(4-Cyclopropoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
1g
$ 330.00

Crysdot
2-(4-Cyclopropoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
5g
$ 1179.00

Chemcia Scientific
2-(4-Cyclopropoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane
1 G
$ 335.00

AK Scientific
2-(4-Cyclopropoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
1g
$ 517.00

Total 8 raw suppliers

Chemical Property of 2-(4-Cyclopropoxy-phenyl)-4,4,5,5-tetraMethyl-[1,3,2]dioxaborolane

Chemical Property:

Boiling Point:360.6±25.0 °C(Predicted)
PSA：27.69000
Density:1.07±0.1 g/cm3(Predicted)
LogP:2.52700

Purity/Quality:

99%,98%, ^*data from raw suppliers

2-(4-Cyclopropoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 2-(4-Cyclopropoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Technology Process of 2-(4-Cyclopropoxy-phenyl)-4,4,5,5-tetraMethyl-[1,3,2]dioxaborolane

There total 1 articles about 2-(4-Cyclopropoxy-phenyl)-4,4,5,5-tetraMethyl-[1,3,2]dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 38380-85-7
1-bromo-4-(cyclopropyloxy)benzene

: 73183-34-3
bis(pinacol)diborane

: 1398503-71-3
2-(4-cyclopropoxyphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: With potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In dimethyl sulfoxide; at 80 ℃; for 5h; Inert atmosphere;

Reference yield: 84.0%

: 1398503-71-3
2-(4-cyclopropoxyphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 4-cyclopropoxyphenol

Guidance literature:: With 4-methylmorpholine N-oxide; In tetrahydrofuran; at 20 - 75 ℃; for 19.5h;

Reference yield: 13.0%

: 625-92-3
3,5-dibromopyridine

: 1398503-71-3
2-(4-cyclopropoxyphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 76-05-1
trifluoroacetic acid

: 123088-59-5
4-carbamoylphenylboronic acid

: 4-(5-(4-cyclopropoxyphenyl)pyridin-3-yl)benzamide trifluoroacetic acid salt

Guidance literature:: 3,5-dibromopyridine; 2-(4-cyclopropoxyphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In tetrahydrofuran; at 70 ℃; for 18h; Inert atmosphere;

4-carbamoylphenylboronic acid; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In tetrahydrofuran; at 70 ℃; for 18h; Inert atmosphere;

trifluoroacetic acid;
DOI:10.1021/acsmedchemlett.5b00215