TOLUENE-13C6

Base Information

• Chemical Name: TOLUENE-13C6
• CAS No.: 287399-35-3
• Molecular Formula: C7H8
• Molecular Weight: 98.19
• Mol file: 287399-35-3.mol

Synonyms:TOLUENE-13C6;Methyl(benzene-13C6);Toluene-13C6 (phenyl-13C6);Toluene-(phenyl-13C6)

Chemical Property of TOLUENE-13C6

Chemical Property:

• Melting Point: -93 °C(lit.)
• Boiling Point: 110 °C(lit.)
• PSA: 0.00000
• Density: 0.920 g/mL at 25 °C
• LogP: 1.99500

Purity/Quality:

99%13C ^*data from raw suppliers

Toluene-13C6 ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F,Xn
• Statements: 11-38-48/20-63-65-67
• Safety Statements: 36/37-46-62

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TOLUENE-13C6

There total 2 articles about TOLUENE-13C6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[13C]methanol (14742-26-8) → 13C7-toluene (287399-36-4,287399-35-3) + U-(13)C-naphthalene (219526-41-7,287399-39-7)

Guidance literature:

With H-GaAl-ZSM-5 zeolite; at 550 ℃;

DOI:10.1002/anie.200500694

Reference yield:

anisole-1,2,3,4,5,6-13C6 (152571-52-3,154492-88-3) → U-(13)C-naphthalene (219526-41-7,287399-39-7) + benzene-(13)C6 (32488-44-1) + [1,2,3,4,5,6-13C6]toluene (287399-35-3)

Guidance literature:

With ZSM-5 zeolite catalyst powder (CBV 2314); In neat (no solvent, gas phase); at 600 ℃; Mechanism;

DOI:10.1039/c5gc02548f

Reference yield:

13C7-toluene (287399-36-4,287399-35-3) + Dimethyl ether (115-10-6,157621-61-9) → 1-butylene (106-98-9,9003-28-5) + 2-methyl-but-2-ene (513-35-9) + methylbutane (78-78-4) + ethene (74-85-1)

Guidance literature:

With H_2.2[Al_2.2Si_93.8O₁₉₂]; at 274.84 ℃; under 975.098 Torr;

DOI:10.1016/j.jcat.2013.03.021

upstream raw materials:

anisole-1,2,3,4,5,6-¹³C₆

[¹³C]methanol

Downstream raw materials:

1-butylene

2-methyl-but-2-ene

methylbutane

ethene

Refernces

• 1、 Choudhary, Vasant R.,Mondal, Kartick C.,Mulla, Shafeek A. R.. "Simultaneous conversion of methane and methanol into gasoline over bifunctional Ga-, Zn-, In-, and/or Mo-modified ZSM-5 zeolites". . p. 4381 - 4385. Retrieved 2007/10/03.