1-Methoxy-3-methyl-2-butanamine hydrochloride

Base Information

Chemical Name:1-Methoxy-3-methyl-2-butanamine hydrochloride
CAS No.:1185294-54-5
Molecular Formula:C6H16ClNO
Molecular Weight:153.65034
Hs Code.:2922199090
Mol file:1185294-54-5.mol

Synonyms:1-Methoxy-3-methyl-2-butanamine hydrochloride;1185294-54-5;1-Methoxy-3-methyl-2-butanaminehydrochloride;1-methoxy-3-methylbutan-2-amine;hydrochloride;1-Methoxy-3-methyl-2-butanamine HCl;1-methoxy-3-methylbutan-2-amine hydrochloride;SCHEMBL1430480;MELMFNVCMMMNKN-UHFFFAOYSA-N;1-Methoxy-3-methylbutan-2-amine HCl;AKOS015849254;AM806372;BS-41700;CS-0038205;1-Methoxy-3-methyl-2-butanamine hydrochloride, AldrichCPR

Suppliers and Price of 1-Methoxy-3-methyl-2-butanamine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-Methoxy-3-methyl-2-butanamineHydrochloride
100mg
$ 155.00

Matrix Scientific
1-Methoxy-3-methyl-2-butanaminehydrochloride
500mg
$ 199.00

American Custom Chemicals Corporation
1-METHOXY-3-METHYL-2-BUTANAMINE HYDROCHLORIDE 95.00%
500MG
$ 795.80

AK Scientific
1-Methoxy-3-methyl-2-butanaminehydrochloride
500mg
$ 318.00

Total 5 raw suppliers

Chemical Property of 1-Methoxy-3-methyl-2-butanamine hydrochloride

Chemical Property:

PSA：35.25000
LogP:2.11840
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:153.0920418
Heavy Atom Count:9
Complexity:54.5

Purity/Quality:

98%min ^*data from raw suppliers

1-Methoxy-3-methyl-2-butanamineHydrochloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C(COC)N.Cl

Technology Process of 1-Methoxy-3-methyl-2-butanamine hydrochloride

There total 1 articles about 1-Methoxy-3-methyl-2-butanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 925-90-6
ethylmagnesium bromide

: 87768-46-5
N-[(1S)-1-(methoxymethyl)-2-methylpropyl]benzamide

: 93-55-0
1-phenyl-propan-1-one

: 1185294-54-5
1-(1-methylethoxy)-3-phenyl-2-propylamine hydrochloride

Guidance literature:: N-[(1S)-1-(methoxymethyl)-2-methylpropyl]benzamide; With 2-fluoropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at 0 ℃; for 0.5h;

ethylmagnesium bromide; With cerium(III) chloride; In tetrahydrofuran; dichloromethane; at -78 ℃; for 2h;

With hydrogenchloride; In ethyl acetate;
DOI:10.1016/j.cclet.2015.05.033

Reference yield:

: 175458-86-3,1185294-54-5
(R)-1-methoxymethyl-2-methyl-propylamine hydrochloride

: 4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(1R-methoxymethyl-2-methyl-propylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one dihydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tris(acetoxy)borohydride / 1-methyl-pyrrolidin-2-one; dichloromethane / 4 h / 20 °C

2.1: dichloromethane / 18 h / 20 °C

3.1: water; acetic acid / tetrahydrofuran / 4.5 h / Heating / reflux

4.1: Dess-Martin periodane / dichloromethane / 1 h

5.1: hydrogenchloride; sodium cyanoborohydride; acetic acid / methanol; diethyl ether / 2.5 h / 0 - 20 °C

6.1: trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C

6.2: 0.08 h / 20 °C

With hydrogenchloride; water; sodium tris(acetoxy)borohydride; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; trifluoroacetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; diethyl ether; dichloromethane;

Reference yield:

: 175458-86-3,1185294-54-5
(R)-1-methoxymethyl-2-methyl-propylamine hydrochloride

: 950504-35-5
(1R-methoxymethyl-2-methyl-propyl)-[3-(2-oxo-ethyl)-benzyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tris(acetoxy)borohydride / 1-methyl-pyrrolidin-2-one; dichloromethane / 4 h / 20 °C

2: dichloromethane / 18 h / 20 °C

3: water; acetic acid / tetrahydrofuran / 4.5 h / Heating / reflux

4: Dess-Martin periodane / dichloromethane / 1 h

With water; sodium tris(acetoxy)borohydride; Dess-Martin periodane; acetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane;