Methane sulfonic acid-d

Base Information

• Chemical Name: Methane sulfonic acid-d
• CAS No.: 66178-40-3
• Molecular Formula: CH4O3S
• Molecular Weight: 97.099
• Mol file: 66178-40-3.mol

Synonyms:Methane sulfonic acid-d

Chemical Property of Methane sulfonic acid-d

Chemical Property:

• PSA: 62.75000
• Density: 1.496 g/mL at 25 °C
• LogP: 0.58480

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methane sulfonic acid-d

There total 5 articles about Methane sulfonic acid-d which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[D3]acetonitrile (2206-26-0) + bis(methanesulfonyl)peroxide (1001-62-3) → O-deuterio-methanesulfonic acid (66178-40-3) + C3H3(2)H2NO3S (130351-44-9) + Methanesulfonic anhydride (7143-01-3)

Guidance literature:

at 30 ℃; for 24h;

DOI:10.1021/j100388a017

Reference yield:

bis(methanesulfonyl)peroxide (1001-62-3) → O-deuterio-methanesulfonic acid (66178-40-3) + C3H3(2)H2NO3S (130351-44-9) + Methanesulfonic anhydride (7143-01-3)

Guidance literature:

In [D₃]acetonitrile; at 30 ℃; Rate constant;

DOI:10.1021/j100388a017

Reference yield:

bis(methanesulfonyl)peroxide (1001-62-3) → methanesulfonic acid (75-75-2,98527-29-8) + methanesulfonyloxyacetonitrile (3586-51-4) + O-deuterio-methanesulfonic acid (66178-40-3) + Methanesulfonic anhydride (7143-01-3)

Guidance literature:

In [D₃]acetonitrile; at 30 ℃; Rate constant; Irradiation;

DOI:10.1021/j100388a017

upstream raw materials:

[D₃]acetonitrile

bis(methanesulfonyl)peroxide

Refernces