N-tert-Butyl-O-[1-[4-(chloroMethyl)phenyl]ethyl]-N-(2-Methyl-1-phenylpropyl)hydroxylaMine

Base Information

Chemical Name:N-tert-Butyl-O-[1-[4-(chloroMethyl)phenyl]ethyl]-N-(2-Methyl-1-phenylpropyl)hydroxylaMine
CAS No.:227000-85-3
Molecular Formula:C23H32ClNO
Molecular Weight:373.966
Hs Code.:
Mol file:227000-85-3.mol

Synonyms:N-tert-Butyl-O-[1-[4-(chloroMethyl)phenyl]ethyl]-N-(2-Methyl-1-phenylpropyl)hydroxylaMine

Suppliers and Price of N-tert-Butyl-O-[1-[4-(chloroMethyl)phenyl]ethyl]-N-(2-Methyl-1-phenylpropyl)hydroxylaMine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-tert-Butyl-O-[1-[4-(chloromethyl)phenyl]ethyl]-N-(2-methyl-1-phenylpropyl)hydroxylamine
250mg
$ 151.00

American Custom Chemicals Corporation
N-TERT-BUTYL-O-[1-[4-(CHLOROMETHYL)PHENYL]ETHYL]-N-(2-METHYL-1-PHENYLPROPYL)HYDROXYLAMINE 95.00%
250MG
$ 667.62

Total 5 raw suppliers

Chemical Property of N-tert-Butyl-O-[1-[4-(chloroMethyl)phenyl]ethyl]-N-(2-Methyl-1-phenylpropyl)hydroxylaMine

Chemical Property:

Melting Point:43-47°C
Boiling Point:461.3±55.0 °C(Predicted)
PKA:2.78±0.70(Predicted)
Flash Point:>110℃
PSA：12.47000
Density:1.043±0.06 g/cm3(Predicted)
LogP:6.91580
Storage Temp.:?20°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-tert-Butyl-O-[1-[4-(chloromethyl)phenyl]ethyl]-N-(2-methyl-1-phenylpropyl)hydroxylamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:O,C
Statements: 8-34
Safety Statements: 17-26-36/37/39-45

MSDS Files:: SDS file from LookChem

Useful:

Uses Block Copolymer Synthesis Using a Commercially Available NMP Inititator

Technology Process of N-tert-Butyl-O-[1-[4-(chloroMethyl)phenyl]ethyl]-N-(2-Methyl-1-phenylpropyl)hydroxylaMine

There total 3 articles about N-tert-Butyl-O-[1-[4-(chloroMethyl)phenyl]ethyl]-N-(2-Methyl-1-phenylpropyl)hydroxylaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.1%

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 61015-94-9
N-(tert-butyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

: 227000-85-3
N-tert-butyl-O-[1-(4-chloromethyl-phenyl)-ethyl]-N-(2-methyl-1-phenyl-propyl)-hydroxylamine

Guidance literature:: With sodium tetrahydroborate; (salen)Mn; In ethanol; benzene; at 20 ℃; for 15h;
DOI:10.1021/ja070748i

Reference yield: 63.1%

: 227000-85-3
N-tert-butyl-O-[1-(4-chloromethyl-phenyl)-ethyl]-N-(2-methyl-1-phenyl-propyl)-hydroxylamine

Guidance literature:

Reference yield:

: 85664-55-7
(Z)-2-methyl-N-(2-methylpropylidene)propan-2-amine N-oxide

: 227000-85-3
N-tert-butyl-O-[1-(4-chloromethyl-phenyl)-ethyl]-N-(2-methyl-1-phenyl-propyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) Cu(OAc)2, conc. aq. NH₃, air / 1.) THF, Et₂O, RT, 12 h, 2.) THF, Et₂O, MeOH, 10 min

2: 62 percent / manganese(III) chloride, di-tert-butyl peroxide, NaBH₄ / toluene; ethanol / 12 h / Ambient temperature

With ammonium hydroxide; sodium tetrahydroborate; copper diacetate; air; [(R,R)-(N,N-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato)]manganese(III) chloride; di-tert-butyl peroxide; In ethanol; toluene;
DOI:10.1021/ja984013c