2,6-Dichloro-9-[2,3-O-(1-Methylethylidene)-Beta-D-ribofuranosyl]-9H-purine

Base Information

• Chemical Name: 2,6-Dichloro-9-[2,3-O-(1-Methylethylidene)-Beta-D-ribofuranosyl]-9H-purine
• CAS No.: 52678-40-7
• Molecular Formula: C13H14Cl2N4O4
• Molecular Weight: 361.185
• Mol file: 52678-40-7.mol

Synonyms:2,6-Dichloro-9-[2,3-O-(1-Methylethylidene)-Beta-D-ribofuranosyl]-9H-purine;1-(2,6-dichloro-purin-9-yl)-O2,O3-isopropylidene-β-D-1-deoxy-ribofuranose

Chemical Property of 2,6-Dichloro-9-[2,3-O-(1-Methylethylidene)-Beta-D-ribofuranosyl]-9H-purine

Chemical Property:

• Boiling Point: 517.3±60.0 °C(Predicted)
• PKA: 14.14±0.10(Predicted)
• PSA: 91.52000
• Density: 1.88±0.1 g/cm3(Predicted)
• LogP: 1.54290

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-Dichloro-9-[2,3-O-(1-Methylethylidene)-Beta-D-ribofuranosyl]-9H-purine

There total 3 articles about 2,6-Dichloro-9-[2,3-O-(1-Methylethylidene)-Beta-D-ribofuranosyl]-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2,2-dimethoxy-propane (77-76-9) + 2,6-dichloropurine riboside (13276-52-3) → [(3aR,4R,6R,6aR)-4-(2,6-dichloropurin-9-yl)-2,2-dimethyl-3a,4,6,6a-tetrahydrofuro[3,4-d][1,3]dioxol-6-yl]methanol (52678-40-7)

Guidance literature:

With toluene-4-sulfonic acid; In acetone; at 20 ℃; for 16h;

Reference yield: 90.0%

acetone (67-64-1) + 2,6-dichloropurine riboside (13276-52-3) → [(3aR,4R,6R,6aR)-4-(2,6-dichloropurin-9-yl)-2,2-dimethyl-3a,4,6,6a-tetrahydrofuro[3,4-d][1,3]dioxol-6-yl]methanol (52678-40-7)

Guidance literature:

With toluene-4-sulfonic acid; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1016/j.jphotobiol.2016.03.055

Reference yield:

→ [(3aR,4R,6R,6aR)-4-(2,6-dichloropurin-9-yl)-2,2-dimethyl-3a,4,6,6a-tetrahydrofuro[3,4-d][1,3]dioxol-6-yl]methanol (52678-40-7)

Guidance literature:

2,6-Dichlor-9-β-D-ribofuranosylpurin, 2,2-Dimethoxypropan, Aceton in Perchlor- saeure;

upstream raw materials:

2,2-dimethoxy-propane

2,6-dichloropurine riboside

acetone

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