1-Bromo-8-methylnaphthalene

Base Information

Chemical Name:1-Bromo-8-methylnaphthalene
CAS No.:33295-37-3
Molecular Formula:C11H9Br
Molecular Weight:221.096
Hs Code.:
European Community (EC) Number:683-744-4
DSSTox Substance ID:DTXSID00401230
Nikkaji Number:J945.081E
Wikidata:Q82204290
Mol file:33295-37-3.mol

Synonyms:1-bromo-8-methylnaphthalene;33295-37-3;1-bromo-8-methyl-naphthalene;MFCD00229485;SCHEMBL5403909;DTXSID00401230;QTWVRVGVJURUFK-UHFFFAOYSA-N;AMY16441;AKOS024322796;CS-16111;SY253837;CS-0088873;FT-0744777;EN300-128953;P20677;Z1269205197

Suppliers and Price of 1-Bromo-8-methylnaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

ChemScene
1-Bromo-8-methylnaphthalene ≥97.0%
1g
$ 200.00

ChemScene
1-Bromo-8-methylnaphthalene ≥97.0%
250mg
$ 100.00

ChemScene
1-Bromo-8-methylnaphthalene ≥97.0%
5g
$ 600.00

Chemenu
1-Bromo-8-methylnaphthalene 95%
5g
$ 536.00

American Custom Chemicals Corporation
1-BROMO-8-METHYLNAPHTHALENE 95.00%
5MG
$ 505.60

Alichem
8-Bromo-1-methylnaphthalene
1g
$ 1651.30

Alichem
8-Bromo-1-methylnaphthalene
500mg
$ 1029.00

Alichem
8-Bromo-1-methylnaphthalene
250mg
$ 652.80

AK Scientific
1-Bromo-8-methylnaphthalene
250mg
$ 627.00

Total 13 raw suppliers

Chemical Property of 1-Bromo-8-methylnaphthalene

Chemical Property:

Melting Point:80 °C(Solv: ethanol (64-17-5))
Boiling Point:115-130 °C(Press: 3.5 Torr)
PSA：0.00000
Density:1.417±0.06 g/cm3(Predicted)
LogP:3.91070
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:219.98876
Heavy Atom Count:12
Complexity:155

Purity/Quality:

97% ^*data from raw suppliers

1-Bromo-8-methylnaphthalene ≥97.0% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C(=CC=C1)C=CC=C2Br

Technology Process of 1-Bromo-8-methylnaphthalene

There total 3 articles about 1-Bromo-8-methylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60-29-7,927820-24-4
diethyl ether

: 4044-58-0
1-bromo-8-iodo-naphthalene

: 569-41-5
1,8-dimethylnaphthalene

: 33295-37-3
1-bromo-8-methylnaphthalene

Guidance literature:: anschliessende Behandlung mit Dimethylsulfat in Benzol bei Siedetemperatur;
DOI:10.1021/ja01870a044

Reference yield:

: 8-bromo-1-methyl-1,4-dihydro-1,4-epoxynaphthalene

: 33295-37-3
1-bromo-8-methylnaphthalene

: 8-bromo-1-methyl-1,2,3,4-tetrahydro-1,4-epoxynaphthalen

: 90-12-0,34475-76-8
1-Methylnaphthalene

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; at 20 ℃;
DOI:10.1021/acs.joc.5b00730

Reference yield:

: 3333-20-8
1-allyl-3-methylbenzene

: 68251-76-3
1-bromo-6-methylnaphthalene

: 33295-37-3
1-bromo-8-methylnaphthalene

Guidance literature:: With carbon tetrabromide; iron; In ethanol; at 20 ℃; for 2h; Overall yield = 88 percent; Overall yield = 195 mg; Irradiation;
DOI:10.1002/adsc.202001249