2-BENZHYDRYL-BENZOOXAZOLE

Base Information

• Chemical Name: 2-BENZHYDRYL-BENZOOXAZOLE
• CAS No.: 73713-90-3
• Molecular Formula: C20H15NO
• Molecular Weight: 285.345
• Mol file: 73713-90-3.mol

Synonyms:2-benzhydryl-benzoxazole;BENZOXAZOLE,2-DIPHENYLMETHYL;2-(diphenylmethyl)-1,3-benzoxazole;2-benzhydrylbenzo[d]oxazole;2-(diphenylmethyl)benzoxazole;2-Benzhydryl-benzoxazol;

Chemical Property of 2-BENZHYDRYL-BENZOOXAZOLE

Chemical Property:

• Vapor Pressure: 1.56E-07mmHg at 25°C
• Boiling Point: 440.1°C at 760 mmHg
• Flash Point: 187.4°C
• PSA: 26.03000
• Density: 1.175g/cm³
• LogP: 5.00800

Purity/Quality:

98% ^*data from raw suppliers

2-BENZHYDRYL-BENZOOXAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-BENZHYDRYL-BENZOOXAZOLE

There total 22 articles about 2-BENZHYDRYL-BENZOOXAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-methyl-1,3-benzoxazole (95-21-6) + chlorobenzene (108-90-7) → α-(2-benzoxazolyl)diphenylmethane (73713-90-3)

Guidance literature:

With palladium diacetate; sodium t-butanolate; tricyclohexylphosphine; In o-xylene; at 130 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol200345a

Reference yield: 89.0%

benzoxazole (273-53-0,29791-96-6) + diphenylmethyl 3,5-bis(trifluoromethyl)phenylsulfone → 1,1,2,2-tetraphenylethane (632-50-8) + α-(2-benzoxazolyl)diphenylmethane (73713-90-3)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,3-bis-(diphenylphosphino)propane; lithium tert-butoxide; In 1,4-dioxane; at 120 ℃; for 12h; Reagent/catalyst; Temperature; Solvent; Catalytic behavior; Sealed tube; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.orglett.7b01510

Reference yield: 80.0%

diphenylacetic acid chloride (1871-76-7) + 2-amino-phenol (95-55-6) → α-(2-benzoxazolyl)diphenylmethane (73713-90-3)

Guidance literature:

With triethylamine; In ethyl acetate; Ambient temperature;

upstream raw materials:

diphenylacetic acid chloride

2-amino-phenol

α-(2-benzoxazolyl)diphenylmethanol

iodobenzene

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