5-Bromobenzene-1,2,3-triamine

Base Information

Chemical Name:5-Bromobenzene-1,2,3-triamine
CAS No.:1121586-23-9
Molecular Formula:C6H8BrN3
Molecular Weight:202.054
Hs Code.:2921590090
DSSTox Substance ID:DTXSID40696769
Wikidata:Q82626467
Mol file:1121586-23-9.mol

Synonyms:5-Bromobenzene-1,2,3-triamine;1121586-23-9;5-Bromo-2,3-Diaminoaniline;SCHEMBL12819217;DTXSID40696769;LKRYFTWIURQFJE-UHFFFAOYSA-N;AKOS015995361

Suppliers and Price of 5-Bromobenzene-1,2,3-triamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
5-Bromobenzene-1,2,3-triamine 95+%
1g
$ 455.00

American Custom Chemicals Corporation
5-BROMOBENZENE-1,2,3-TRIAMINE 95.00%
5MG
$ 503.95

Total 6 raw suppliers

Chemical Property of 5-Bromobenzene-1,2,3-triamine

Chemical Property:

Boiling Point:352.7±37.0 °C(Predicted)
PKA:3.79±0.50(Predicted)
PSA：78.06000
Density:1.796±0.06 g/cm3(Predicted)
LogP:2.93930
Storage Temp.:2-8°C
XLogP3:0.6
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:200.99016
Heavy Atom Count:10
Complexity:108

Purity/Quality:

98%min ^*data from raw suppliers

5-Bromobenzene-1,2,3-triamine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=C(C=C(C(=C1N)N)N)Br

Technology Process of 5-Bromobenzene-1,2,3-triamine

There total 2 articles about 5-Bromobenzene-1,2,3-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.1%

: 62554-90-9
4-bromo-2,6-dinitroaniline

: 1121586-23-9
5-bromobenzene-1,2,3-triamine

Guidance literature:: 4-bromo-2,6-dinitroaniline; With hydrogenchloride; tin(II) chloride dihdyrate; In water; at -20 - 20 ℃;

With water; sodium hydroxide; pH=10;

Reference yield:

: 606-22-4
2,6-dinitroaniline

: 1121586-23-9
5-bromobenzene-1,2,3-triamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: bromine; acetic acid

2.1: hydrogenchloride; tin(II) chloride dihdyrate / water / -20 - 20 °C

2.2: pH 10

With hydrogenchloride; tin(II) chloride dihdyrate; bromine; acetic acid; In water;

Reference yield:

: 1121586-23-9
5-bromobenzene-1,2,3-triamine

: 1401449-66-8
N-cyclopropyl-2-methyl-4-{6-(pyridin-4-yl)-4-[(3,3,3-trifluoropropyl)amino]-1H-benzimidazol-1-yl}benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / 20 °C / Reflux

1.2: pH 8

2.1: pyridine N-oxide; pyridine; copper diacetate / dichloromethane / 20 - 40 °C / Inert atmosphere

3.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

4.1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1-methyl-pyrrolidin-2-one; water / 0.67 h / 140 °C / Microwave irradiation

With pyridine; pyridine N-oxide; hydrogenchloride; copper diacetate; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1-methyl-pyrrolidin-2-one; dichloromethane; water; 1,2-dichloro-ethane;