Bicyclo[2.2.1]heptane-2-carbonyl chloride, 3,3-dimethyl-, (1R-exo)- (9CI)

Base Information

• Chemical Name: Bicyclo[2.2.1]heptane-2-carbonyl chloride, 3,3-dimethyl-, (1R-exo)- (9CI)
• CAS No.: 67596-91-2
• Molecular Formula: C10H15ClO
• Molecular Weight: 186.681

Synonyms:Bicyclo[2.2.1]heptane-2-carbonyl chloride, 3,3-dimethyl-, (1R-exo)- (9CI)

Chemical Property of Bicyclo[2.2.1]heptane-2-carbonyl chloride, 3,3-dimethyl-, (1R-exo)- (9CI)

Chemical Property:

• Boiling Point: 93 - 95 °C (11 mmHg)
• PSA: 17.07000
• LogP: 2.82410

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]heptane-2-carbonyl chloride, 3,3-dimethyl-, (1R-exo)- (9CI)

There total 4 articles about Bicyclo[2.2.1]heptane-2-carbonyl chloride, 3,3-dimethyl-, (1R-exo)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-exo-10-camphanoic acid (67519-00-0) → (+/-)-isocamphenilanic acid-chloride (61175-88-0,67596-91-2,85440-78-4)

Guidance literature:

With oxalyl dichloride; In hexane; 1) 0 deg C to rt, 2) reflux, 1-2 h;

DOI:10.1021/jo00004a019

Reference yield:

→ (+/-)-isocamphenilanic acid-chloride (61175-88-0,67596-91-2,85440-78-4)

Guidance literature:

With phosphorus trichloride;

Reference yield:

endo-2,2-dimethylbicyclo<2.2.1>heptane-3-carboxylic acid (85506-67-8) → (+/-)-isocamphenilanic acid-chloride (61175-88-0,67596-91-2,85440-78-4)

Guidance literature:

With phosphorus pentachloride; Petroleum ether;

upstream raw materials:

endo-2,2-dimethylbicyclo<2.2.1>heptane-3-carboxylic acid

2-exo-10-camphanoic acid

Downstream raw materials:

3-((1S,2R,4R)-3,3-Dimethyl-bicyclo[2.2.1]hept-2-yl)-propionyl chloride

3-((1R,2R,4S)-3,3-Dimethyl-bicyclo[2.2.1]hept-2-yl)-propionyl chloride

2,6-Dimethyltricyclo<5.2.1.0^2,6>decan-3-one Tosylhydrazone

(1S,2R,4R)-2-Methyl-3-methylene-2-(4-methyl-pent-3-enyl)-bicyclo[2.2.1]heptane

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