ethyl 6-bromo-1,2-dihydro-3-methoxy-1-methyl-2-oxopyridine-4-carboxylate

Base Information

Chemical Name:ethyl 6-bromo-1,2-dihydro-3-methoxy-1-methyl-2-oxopyridine-4-carboxylate
CAS No.:1429204-40-9
Molecular Formula:C10H12BrNO4
Molecular Weight:290.114
Hs Code.:

Synonyms:ethyl 6-bromo-1,2-dihydro-3-methoxy-1-methyl-2-oxopyridine-4-carboxylate

Suppliers and Price of ethyl 6-bromo-1,2-dihydro-3-methoxy-1-methyl-2-oxopyridine-4-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Ethyl6-bromo-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylate 95+%
1g
$ 673.00

Alichem
Ethyl6-bromo-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylate
1g
$ 751.80

Total 2 raw suppliers

Chemical Property of ethyl 6-bromo-1,2-dihydro-3-methoxy-1-methyl-2-oxopyridine-4-carboxylate

Chemical Property:

PSA：57.53000
LogP:1.33310

Purity/Quality:

97% ^*data from raw suppliers

Ethyl6-bromo-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 6-bromo-1,2-dihydro-3-methoxy-1-methyl-2-oxopyridine-4-carboxylate

There total 1 articles about ethyl 6-bromo-1,2-dihydro-3-methoxy-1-methyl-2-oxopyridine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.2%

: 130879-43-5
3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylic acid ethyl ester

: 1429204-40-9
ethyl 6-bromo-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylate

Guidance literature:: With N-Bromosuccinimide; In 1,2-dichloro-ethane; at 20 ℃;

Reference yield: 58.5%

: 159020-59-4
(3-fluoro-5-(trifluoromethyl)phenyl)boronic acid

: 1429204-40-9
ethyl 6-bromo-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylate

: 1429204-52-3
ethyl 6-(3-fluoro-5-(trifluoromethyl)phenyl)-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; at 160 ℃; for 0.5h; Inert atmosphere; Microwave irradiation; Sealed tube;

Reference yield:

: 1429204-40-9
ethyl 6-bromo-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylate

: 1429204-53-4
6-(3-fluoro-5-(trifluoromethyl)phenyl)-3-methoxy-1-methyl-2-oxo-1,2-dihydropyridine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.5 h / 160 °C / Inert atmosphere; Microwave irradiation; Sealed tube

2: lithium hydroxide / water; tetrahydrofuran; methanol / 65 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water;