N-((5-bromopyridin-3-yl)methyl)-2-methoxyethanamine

Base Information

• Chemical Name: N-((5-bromopyridin-3-yl)methyl)-2-methoxyethanamine
• CAS No.: 1246034-49-0
• Molecular Formula: C₉H₁₃BrN₂O
• Molecular Weight: 245.119
• Hs Code.: 2933399090
• Mol file: 1246034-49-0.mol

Synonyms:N-((5-bromopyridin-3-yl)methyl)-2-methoxyethanamine;5-bromo-N-(2-methoxyethyl)-3-Pyridinemethan amine

Chemical Property of N-((5-bromopyridin-3-yl)methyl)-2-methoxyethanamine

Chemical Property:

• PSA: 34.15000
• LogP: 1.97100
• Storage Temp.: 2-8°C

Purity/Quality:

95+% ^*data from raw suppliers

N-((5-Bromopyridin-3-yl)methyl)-2-methoxyethanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-((5-bromopyridin-3-yl)methyl)-2-methoxyethanamine

There total 1 articles about N-((5-bromopyridin-3-yl)methyl)-2-methoxyethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-bromo-5-(chloromethyl)-pyridine hydrochloride (39741-46-3) + 2-methoxyethylamine (109-85-3) → [(5-bromo-3-pyridinyl)methyl][2-(methyloxy)ethyl]amine (1246034-49-0)

Guidance literature:

With potassium carbonate; In acetonitrile; at 80 ℃; for 4h;

Reference yield: 100.0%

[(5-bromo-3-pyridinyl)methyl][2-(methyloxy)ethyl]amine (1246034-49-0) + bis(pinacol)diborane (73183-34-3) → [2-(methyloxy)ethyl]{[5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-pyridinyl]methyl}amine (919347-14-1)

Guidance literature:

With potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In acetonitrile; at 160 ℃; for 0.25h; Sealed tube; Microwave irradiation;

upstream raw materials:

3-bromo-5-(chloromethyl)-pyridine hydrochloride

2-methoxyethylamine

Downstream raw materials:

[2-(methyloxy)ethyl]{[5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-pyridinyl]methyl}amine

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